5-(3-Methyl-1,6-diphenyl-1H-pyrazolo[3,4-b]pyrazin-5-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol

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Chemical Name:5-(3-Methyl-1,6-diphenyl-1H-pyrazolo[3,4-b]pyrazin-5-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol
CAS No.:214914-46-2
Molecular Formula:C₂₆H₁₉N₇S
Molecular Weight:461.55
Hs Code.:

Synonyms:5-(3-Methyl-1,6-diphenyl-1H-pyrazolo[3,4-b]pyrazin-5-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol

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Chemical Property of 5-(3-Methyl-1,6-diphenyl-1H-pyrazolo[3,4-b]pyrazin-5-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol

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Technology Process of 5-(3-Methyl-1,6-diphenyl-1H-pyrazolo[3,4-b]pyrazin-5-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol

There total 8 articles about 5-(3-Methyl-1,6-diphenyl-1H-pyrazolo[3,4-b]pyrazin-5-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 214914-44-0
1-Phenyl-4-(1,6-diphenyl-3-methyl-1H-pyrazolo[3,4-b]pyrazin-5-oyl)thiosemicarbazide

: 214914-46-2
5-(3-Methyl-1,6-diphenyl-1H-pyrazolo[3,4-b]pyrazin-5-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol

Guidance literature:: With sodium hydroxide; water; for 3h; Heating;
DOI:10.1016/S0014-827X(98)00014-7

Reference yield:

: 52943-85-8
5-amino-3-methyl-4-nitroso-1-phenylpyrazole

: 214914-46-2
5-(3-Methyl-1,6-diphenyl-1H-pyrazolo[3,4-b]pyrazin-5-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol

Guidance literature:: Multi-step reaction with 6 steps

1: 77 percent / pyridine / 3 h / Heating

2: 56 percent / NaOH, H₂O / ethanol / 6 h / Heating

3: 75 percent / H₂SO₄ / 5 h / Heating

4: 76 percent / N₂H₄*H₂O / ethanol / 1 h / Heating

5: 94 percent / ethanol / 0.5 h / Heating

6: 65 percent / NaOH, H₂O / 3 h / Heating

With pyridine; sodium hydroxide; sulfuric acid; water; hydrazine hydrate; In ethanol;
DOI:10.1016/S0014-827X(98)00014-7

Reference yield:

: 614-16-4
Benzoylacetonitrile

: 214914-46-2
5-(3-Methyl-1,6-diphenyl-1H-pyrazolo[3,4-b]pyrazin-5-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol

Guidance literature:: Multi-step reaction with 6 steps

1: 77 percent / pyridine / 3 h / Heating

2: 56 percent / NaOH, H₂O / ethanol / 6 h / Heating

3: 75 percent / H₂SO₄ / 5 h / Heating

4: 76 percent / N₂H₄*H₂O / ethanol / 1 h / Heating

5: 94 percent / ethanol / 0.5 h / Heating

6: 65 percent / NaOH, H₂O / 3 h / Heating

With pyridine; sodium hydroxide; sulfuric acid; water; hydrazine hydrate; In ethanol;
DOI:10.1016/S0014-827X(98)00014-7