1,3-bis{(N₁'-[3'',4''-bis(hydroxy)benzoyl]-N₄'-acetyl)spermidinyl} citrate

Base Information

Chemical Name:1,3-bis{(N₁'-[3'',4''-bis(hydroxy)benzoyl]-N₄'-acetyl)spermidinyl} citrate
CAS No.:1608483-35-7
Molecular Formula:C₃₈H₅₄N₆O₁₃
Molecular Weight:802.879
Hs Code.:

1,3-bis{(N<sub>1</sub>'-[3'',4''-bis(hydroxy)benzoyl]-N<sub>4</sub>'-acetyl)spermidinyl} citrate

Synonyms:1,3-bis{(N₁'-[3'',4''-bis(hydroxy)benzoyl]-N₄'-acetyl)spermidinyl} citrate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-bis{(N₁'-[3'',4''-bis(hydroxy)benzoyl]-N₄'-acetyl)spermidinyl} citrate

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Technology Process of 1,3-bis{(N₁'-[3'',4''-bis(hydroxy)benzoyl]-N₄'-acetyl)spermidinyl} citrate

There total 5 articles about 1,3-bis{(N₁'-[3'',4''-bis(hydroxy)benzoyl]-N₄'-acetyl)spermidinyl} citrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1608483-56-2
C₆₆H₇₈N₆O₁₃

: 1608483-35-7
1,3-bis{(N₁'-[3'',4''-bis(hydroxy)benzoyl]-N₄'-acetyl)spermidinyl} citrate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; water; at 20 ℃; for 36h; under 33753.4 Torr;
DOI:10.1002/ejoc.201301340

Reference yield:

: C₆₇H₈₀N₆O₁₃

: 1608483-35-7
1,3-bis{(N₁'-[3'',4''-bis(hydroxy)benzoyl]-N₄'-acetyl)spermidinyl} citrate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; water; at 20 ℃; for 36h; under 33753.4 Torr; Inert atmosphere; Darkness;
DOI:10.1002/ejoc.201301340

Reference yield:

: 83966-24-9
2-Hydroxy-1,2,3-propanetricarboxylic Acid 2-Isopropyl Ester

: 1608483-35-7
1,3-bis{(N₁'-[3'',4''-bis(hydroxy)benzoyl]-N₄'-acetyl)spermidinyl} citrate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dicyclohexyl-carbodiimide / acetonitrile / 20 h / 20 °C / Inert atmosphere

2.1: triethylamine / N,N-dimethyl-formamide / 0.25 h / Cooling with ice; Inert atmosphere; Darkness

2.2: 20 °C / Molecular sieve; Cooling with ice; Ionic liquid; Darkness

3.1: lithium hydroxide / water; tetrahydrofuran / 0.67 h / 0 °C / Inert atmosphere; Darkness

3.2: strongly acidic ion exchange resin (Dowex50WX8-100, 50–100 mesh) / 0.17 h / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / ethanol; water / 36 h / 20 °C / 33753.4 Torr

With palladium 10% on activated carbon; hydrogen; triethylamine; dicyclohexyl-carbodiimide; lithium hydroxide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/ejoc.201301340