(S)-methyl 2-(2-nitrophenylsulfonamido)-3-(2-(1-phenylvinyl)-1H-indol-3-yl)propanoate

Base Information

Chemical Name:(S)-methyl 2-(2-nitrophenylsulfonamido)-3-(2-(1-phenylvinyl)-1H-indol-3-yl)propanoate
CAS No.:1377936-62-3
Molecular Formula:C₂₆H₂₃N₃O₆S
Molecular Weight:505.551
Hs Code.:

Synonyms:(S)-methyl 2-(2-nitrophenylsulfonamido)-3-(2-(1-phenylvinyl)-1H-indol-3-yl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 2-(2-nitrophenylsulfonamido)-3-(2-(1-phenylvinyl)-1H-indol-3-yl)propanoate

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Technology Process of (S)-methyl 2-(2-nitrophenylsulfonamido)-3-(2-(1-phenylvinyl)-1H-indol-3-yl)propanoate

There total 1 articles about (S)-methyl 2-(2-nitrophenylsulfonamido)-3-(2-(1-phenylvinyl)-1H-indol-3-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 856865-61-7
N-(o-nitrobenzenesulfonyl)-L-tryptophan methyl ester

: 536-74-3
phenylacetylene

: 1377936-62-3
(S)-methyl 2-(2-nitrophenylsulfonamido)-3-(2-(1-phenylvinyl)-1H-indol-3-yl)propanoate

Guidance literature:: With mercuric triflate; In dichloromethane; at 20 ℃; for 3.5h; regioselective reaction;
DOI:10.1039/c2ob25236h

Reference yield:

: 1377936-62-3
(S)-methyl 2-(2-nitrophenylsulfonamido)-3-(2-(1-phenylvinyl)-1H-indol-3-yl)propanoate

: C₂₀H₂₀N₂O₂

Guidance literature:: With caesium carbonate; thiophenol; In acetonitrile; at 0 - 20 ℃; for 3h;
DOI:10.1039/c2ob25236h

Reference yield:

: 1377936-62-3
(S)-methyl 2-(2-nitrophenylsulfonamido)-3-(2-(1-phenylvinyl)-1H-indol-3-yl)propanoate

: C₃₀H₂₇F₃N₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; thiophenol / acetonitrile / 3 h / 0 - 20 °C

2: triethylamine / dichloromethane / 1.25 h / 0 °C

With caesium carbonate; thiophenol; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1039/c2ob25236h