5,5-Dimethyl-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-[1,3]dioxane

Base Information

Chemical Name:5,5-Dimethyl-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-[1,3]dioxane
CAS No.:370104-66-8
Molecular Formula:C₅₆H₉₄O₅
Molecular Weight:847.359
Hs Code.:

Synonyms:5,5-Dimethyl-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-[1,3]dioxane

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Chemical Property of 5,5-Dimethyl-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-[1,3]dioxane

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Technology Process of 5,5-Dimethyl-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-[1,3]dioxane

There total 1 articles about 5,5-Dimethyl-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-[1,3]dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 38252-14-1
5,5-Dimethyl-2--dioxan-(1,3)

: 117241-34-6
(E)-N-phenyl-3,4,5-tris(dodecyloxy)benzaldimine

: 370104-66-8
5,5-Dimethyl-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-[1,3]dioxane

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide; at 85 ℃; for 1h;
DOI:10.1021/jo0106142

Reference yield: 94.0%

: 370104-66-8
5,5-Dimethyl-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-[1,3]dioxane

: 253598-62-8
(E)-4-[2-(3,4,5-tridodecyloxyphenyl)ethenyl]benzaldehyde

Guidance literature:: With trifluoroacetic acid; In dichloromethane; water; at 20 ℃; for 5h;
DOI:10.1021/jo0106142

Reference yield:

: 370104-66-8
5,5-Dimethyl-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-[1,3]dioxane

: C₆₄H₁₀₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / CF₃COOH / CH₂Cl₂; H₂O / 5 h / 20 °C

2: 83 percent / t-BuOK / tetrahydrofuran / 1 h / 20 °C

3: 23 percent / Pd(OAc)2; tri-o-tolylphosphine / xylene; triethylamine / 48 h / 140 °C

With palladium diacetate; potassium tert-butylate; tris-(o-tolyl)phosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; triethylamine; xylene; 3: Heck coupling;
DOI:10.1021/jo0106142