benzyl N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N₂-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetyl glycinate

Base Information

• Chemical Name: benzyl N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N₂-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetyl glycinate
• CAS No.: 1056015-81-6
• Molecular Formula: C₄₇H₄₈N₆O₉
• Molecular Weight: 840.933

Synonyms:benzyl N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N₂-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetyl glycinate

Chemical Property of benzyl N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N₂-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetyl glycinate

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Technology Process of benzyl N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N₂-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetyl glycinate

There total 1 articles about benzyl N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N₂-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetyl glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

benzyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]glycinate (791778-61-5) + 2-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetic acid (1056015-80-5) → benzyl N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N2-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetyl glycinate (1056015-81-6)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 4 - 20 ℃; for 24.2h;

DOI:10.1021/ja804233g

Reference yield: 84.0%

benzyl N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N2-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetyl glycinate (1056015-81-6) → N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N2-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetyl glycine (1056015-82-7)

Guidance literature:

With 1% Pd/C; hydrogen; In methanol; for 2h;

DOI:10.1021/ja804233g

upstream raw materials:

benzyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]glycinate

2-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetic acid

Downstream raw materials:

N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N₂-(6-(2-(2-(tert-butyloxycarbonylamino)ethoxy)phenyl)pyrrolocytosin-1-yl)acetyl glycine

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