anti,anti-9-<4-(methoxycarbonyl)phenyl>-9-methyl-3,6-dioxatetracyclo<6.1.0.0^2,4.0^5,7>nonane

Base Information

• Chemical Name: anti,anti-9-<4-(methoxycarbonyl)phenyl>-9-methyl-3,6-dioxatetracyclo<6.1.0.0^2,4.0^5,7>nonane
• CAS No.: 86318-30-1
• Molecular Formula: C₁₆H₁₆O₄
• Molecular Weight: 272.301

Synonyms:anti,anti-9-<4-(methoxycarbonyl)phenyl>-9-methyl-3,6-dioxatetracyclo<6.1.0.0^2,4.0^5,7>nonane

Chemical Property of anti,anti-9-<4-(methoxycarbonyl)phenyl>-9-methyl-3,6-dioxatetracyclo<6.1.0.0^2,4.0^5,7>nonane

Chemical Property:

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Technology Process of anti,anti-9-<4-(methoxycarbonyl)phenyl>-9-methyl-3,6-dioxatetracyclo<6.1.0.0^2,4.0^5,7>nonane

There total 5 articles about anti,anti-9-<4-(methoxycarbonyl)phenyl>-9-methyl-3,6-dioxatetracyclo<6.1.0.0^2,4.0^5,7>nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

endo-3-<4-(methoxycarbonyl)phenyl>-exo-3-methyl-6,7-dioxatricyclo<3.2.2.02,4>non-8-ene (86318-27-6) → anti,anti-9-<4-(methoxycarbonyl)phenyl>-9-methyl-3,6-dioxatetracyclo<6.1.0.02,4.05,7>nonane (86318-30-1)

Guidance literature:

In tetrachloromethane; at 60 ℃;

Reference yield:

1-bromo-4-(cyclohepta-2,4,6-trien-1-yl)benzene (54615-31-5) → anti,anti-9-<4-(methoxycarbonyl)phenyl>-9-methyl-3,6-dioxatetracyclo<6.1.0.02,4.05,7>nonane (86318-30-1)

Guidance literature:

Multi-step reaction with 5 steps

1: 43 percent / 15percent n-BuLi / diethyl ether; hexane / 0 °C

2: 1) KNH₂ / 1) ether, liquid NH₃, -33 deg C, 2) ether, liquid NH₃

3: 84 percent / diethyl ether / Ambient temperature

4: 54 percent / tetraphenylporphine, O₂ / CH₂Cl₂ / 3 h / -20 °C / Irradiation

5: 93 percent / CCl₄ / 60 °C

With n-butyllithium; oxygen; 5,15,10,20-tetraphenylporphyrin; potassium amide; In tetrachloromethane; diethyl ether; hexane; dichloromethane;

Reference yield:

4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid (86318-22-1) → anti,anti-9-<4-(methoxycarbonyl)phenyl>-9-methyl-3,6-dioxatetracyclo<6.1.0.02,4.05,7>nonane (86318-30-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 1) KNH₂ / 1) ether, liquid NH₃, -33 deg C, 2) ether, liquid NH₃

2: 84 percent / diethyl ether / Ambient temperature

3: 54 percent / tetraphenylporphine, O₂ / CH₂Cl₂ / 3 h / -20 °C / Irradiation

4: 93 percent / CCl₄ / 60 °C

With oxygen; 5,15,10,20-tetraphenylporphyrin; potassium amide; In tetrachloromethane; diethyl ether; dichloromethane;

upstream raw materials:

endo-3-<4-(methoxycarbonyl)phenyl>-exo-3-methyl-6,7-dioxatricyclo<3.2.2.0^2,4>non-8-ene

1-bromo-4-(cyclohepta-2,4,6-trien-1-yl)benzene

4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid

7-(4-carboxyphenyl)-7-methyl-1,3,5-cycloheptatriene

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