C₂₄H₂₆N₆O₃

Base Information

Chemical Name:C₂₄H₂₆N₆O₃
CAS No.:1431701-09-5
Molecular Formula:C₂₄H₂₆N₆O₃
Molecular Weight:446.509
Hs Code.:

C<sub>24</sub>H<sub>26</sub>N<sub>6</sub>O<sub>3</sub>

Synonyms:C₂₄H₂₆N₆O₃

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Chemical Property of C₂₄H₂₆N₆O₃

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Technology Process of C₂₄H₂₆N₆O₃

There total 8 articles about C₂₄H₂₆N₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1431703-33-1
C₂₆H₂₈N₆O₄

: 1431701-09-5
C₂₄H₂₆N₆O₃

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at 5 - 20 ℃; for 36h;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1431701-09-5
C₂₄H₂₆N₆O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / dimethyl sulfoxide / 5 h / 65 °C / Inert atmosphere

5.1: potassium carbonate; methanol / 2 h / 20 °C

6.1: N-ethyl-N,N-diisopropylamine; copper(l) iodide / tetrahydrofuran / 3 h / 5 - 20 °C

7.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 36 h / 5 - 20 °C

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium diacetate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1431701-09-5
C₂₄H₂₆N₆O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / dimethyl sulfoxide / 5 h / 65 °C / Inert atmosphere

5.1: potassium carbonate; methanol / 2 h / 20 °C

6.1: N-ethyl-N,N-diisopropylamine; copper(l) iodide / tetrahydrofuran / 3 h / 5 - 20 °C

7.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 36 h / 5 - 20 °C

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium diacetate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; dimethyl sulfoxide; N,N-dimethyl-formamide;