(S)-1-(4,4'-dimethoxytriphenylmethyloxy)-5-indolo[2,3-b]quinoxalin-6-yl-pentan-2-ol

Base Information

Chemical Name:(S)-1-(4,4'-dimethoxytriphenylmethyloxy)-5-indolo[2,3-b]quinoxalin-6-yl-pentan-2-ol
CAS No.:917077-05-5
Molecular Formula:C₄₀H₃₇N₃O₄
Molecular Weight:623.751
Hs Code.:

Synonyms:(S)-1-(4,4'-dimethoxytriphenylmethyloxy)-5-indolo[2,3-b]quinoxalin-6-yl-pentan-2-ol

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Chemical Property of (S)-1-(4,4'-dimethoxytriphenylmethyloxy)-5-indolo[2,3-b]quinoxalin-6-yl-pentan-2-ol

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Technology Process of (S)-1-(4,4'-dimethoxytriphenylmethyloxy)-5-indolo[2,3-b]quinoxalin-6-yl-pentan-2-ol

There total 4 articles about (S)-1-(4,4'-dimethoxytriphenylmethyloxy)-5-indolo[2,3-b]quinoxalin-6-yl-pentan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 917076-94-9
(S)-5-(indolo[2,3-b]quinoxalin-6-yl)-pentane-1,2-diol

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 917077-05-5
(S)-1-(4,4'-dimethoxytriphenylmethyloxy)-5-indolo[2,3-b]quinoxalin-6-yl-pentan-2-ol

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 36h;
DOI:10.1016/j.tet.2006.09.017

Reference yield:

: 916502-54-0
methanesulfonic acid 3-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-propyl ester

: 917077-05-5
(S)-1-(4,4'-dimethoxytriphenylmethyloxy)-5-indolo[2,3-b]quinoxalin-6-yl-pentan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / NaH / dimethylformamide; various solvent(s) / 80 °C

2: 88 percent / acetic acid / H₂O / 20 °C

3: 34 percent / Et₃N / CH₂Cl₂ / 36 h / 20 °C

With sodium hydride; acetic acid; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2006.09.017

Reference yield:

: 917077-01-1
6-[3-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)propyl]-6H-indolo[2,3-b]quinoxaline

: 917077-05-5
(S)-1-(4,4'-dimethoxytriphenylmethyloxy)-5-indolo[2,3-b]quinoxalin-6-yl-pentan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / acetic acid / H₂O / 20 °C

2: 34 percent / Et₃N / CH₂Cl₂ / 36 h / 20 °C

With acetic acid; triethylamine; In dichloromethane; water;
DOI:10.1016/j.tet.2006.09.017