2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)ethanal

Base Information

Chemical Name:2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)ethanal
CAS No.:1018479-89-4
Molecular Formula:C₂₈H₄₀O₇
Molecular Weight:488.621
Hs Code.:

Synonyms:2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)ethanal

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Chemical Property of 2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)ethanal

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Technology Process of 2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)ethanal

There total 1 articles about 2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)ethanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1018479-97-4
2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)ethan-1-ol

: 1018479-89-4
2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)ethanal

Guidance literature:: With dipyridinium dichromate; sodium acetate; In dichloromethane; at 20 ℃; for 2h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ol800101v

Reference yield: 27.0%

: 22037-28-1
3-bromofurane

: 1018479-89-4
2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)ethanal

: 1018479-90-7
(1S)-2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)-1-(3-furyl)ethan-1-ol

: 1018479-91-8
(1R)-2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)-1-(3-furyl)ethan-1-ol

Guidance literature:: 3-bromofurane; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.5h; Inert atmosphere;

2-((10S,2R,3R,6R,7R)-3,7-di(1,3-dioxolan-2-yl)-10-[(4-methoxyphenyl)methoxy]-2,6-dimethylbicyclo[4.4.0]dec-2-yl)ethanal; In tetrahydrofuran; at -78 ℃; for 0.416667h; Inert atmosphere;
DOI:10.1021/ol800101v