3,4,5,6-tetrahydro-(4S,5S)-2-[(2-bromo)benzyl]-7-[(2-phenethyl)benzyl]-4,5-O-isopropylidene-1,2,7-thiadiazepine 1,1-dioxide

Base Information

Chemical Name:3,4,5,6-tetrahydro-(4S,5S)-2-[(2-bromo)benzyl]-7-[(2-phenethyl)benzyl]-4,5-O-isopropylidene-1,2,7-thiadiazepine 1,1-dioxide
CAS No.:1233878-62-0
Molecular Formula:C₂₉H₃₃BrN₂O₄S
Molecular Weight:585.562
Hs Code.:

Synonyms:3,4,5,6-tetrahydro-(4S,5S)-2-[(2-bromo)benzyl]-7-[(2-phenethyl)benzyl]-4,5-O-isopropylidene-1,2,7-thiadiazepine 1,1-dioxide

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Chemical Property of 3,4,5,6-tetrahydro-(4S,5S)-2-[(2-bromo)benzyl]-7-[(2-phenethyl)benzyl]-4,5-O-isopropylidene-1,2,7-thiadiazepine 1,1-dioxide

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Technology Process of 3,4,5,6-tetrahydro-(4S,5S)-2-[(2-bromo)benzyl]-7-[(2-phenethyl)benzyl]-4,5-O-isopropylidene-1,2,7-thiadiazepine 1,1-dioxide

There total 1 articles about 3,4,5,6-tetrahydro-(4S,5S)-2-[(2-bromo)benzyl]-7-[(2-phenethyl)benzyl]-4,5-O-isopropylidene-1,2,7-thiadiazepine 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 891143-53-6
(4S,5S)-3,4,5,6-tetrahydro-2-(2-bromobenzyl)-4,5-O-isopropylidene-1,2,7-thiadiazepine 1,1-dioxide

: 35388-31-9
2-phenethylbenzyl bromide

: 1233878-62-0
3,4,5,6-tetrahydro-(4S,5S)-2-[(2-bromo)benzyl]-7-[(2-phenethyl)benzyl]-4,5-O-isopropylidene-1,2,7-thiadiazepine 1,1-dioxide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 2h; Sealed vessel;
DOI:10.1016/j.tet.2010.04.023

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1233878-62-0
3,4,5,6-tetrahydro-(4S,5S)-2-[(2-bromo)benzyl]-7-[(2-phenethyl)benzyl]-4,5-O-isopropylidene-1,2,7-thiadiazepine 1,1-dioxide

: C₃₇H₄₀N₂O₄S

Guidance literature:: With palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In water; N,N-dimethyl-formamide; at 150 ℃; for 0.333333h; Microwave irradiation;
DOI:10.1016/j.tet.2010.04.023