(Z)-3-methyl-1-phenylindeno[2,1-e]pyrazolo[3,4-b]pyrazin-5(1H)-one-oxime

Base Information

Chemical Name:(Z)-3-methyl-1-phenylindeno[2,1-e]pyrazolo[3,4-b]pyrazin-5(1H)-one-oxime
CAS No.:1430324-17-6
Molecular Formula:C₁₉H₁₃N₅O
Molecular Weight:327.345
Hs Code.:

Synonyms:(Z)-3-methyl-1-phenylindeno[2,1-e]pyrazolo[3,4-b]pyrazin-5(1H)-one-oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-methyl-1-phenylindeno[2,1-e]pyrazolo[3,4-b]pyrazin-5(1H)-one-oxime

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Technology Process of (Z)-3-methyl-1-phenylindeno[2,1-e]pyrazolo[3,4-b]pyrazin-5(1H)-one-oxime

There total 6 articles about (Z)-3-methyl-1-phenylindeno[2,1-e]pyrazolo[3,4-b]pyrazin-5(1H)-one-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1380215-11-1
3-methyl-1-phenyl-1H-indeno[2,1-e]pyrazolo[3,4-b]pyrazin-5-one

: 1430324-17-6
(Z)-3-methyl-1-phenylindeno[2,1-e]pyrazolo[3,4-b]pyrazin-5(1H)-one-oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; for 3h; Reflux;
DOI:10.1016/j.ejmech.2013.01.025

Reference yield:

: 52943-85-8
5-amino-3-methyl-4-nitroso-1-phenylpyrazole

: 1430324-17-6
(Z)-3-methyl-1-phenylindeno[2,1-e]pyrazolo[3,4-b]pyrazin-5(1H)-one-oxime

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 3 h / Reflux

2: water; sodium hydroxide / 6 h / Reflux

3: thionyl chloride / 2 h / Reflux

4: aluminum (III) chloride; carbon disulfide / 6 h / Reflux

5: pyridine; hydroxylamine hydrochloride / 3 h / Reflux

With pyridine; carbon disulfide; aluminum (III) chloride; thionyl chloride; hydroxylamine hydrochloride; water; sodium hydroxide; 4: |Friedel-Crafts Acylation;
DOI:10.1016/j.ejmech.2013.01.025

Reference yield:

: 214914-37-1
3-Methyl-1,6-diphenyl-1H-pyrazolo[3,4-b]pyrazine-5-carbonyl chloride

: 1430324-17-6
(Z)-3-methyl-1-phenylindeno[2,1-e]pyrazolo[3,4-b]pyrazin-5(1H)-one-oxime

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride; carbon disulfide / 6 h / Reflux

2: pyridine; hydroxylamine hydrochloride / 3 h / Reflux

With pyridine; carbon disulfide; aluminum (III) chloride; hydroxylamine hydrochloride; 1: |Friedel-Crafts Acylation;
DOI:10.1016/j.ejmech.2013.01.025