C₁₇H₂₄O₄

Base Information

• Chemical Name: C₁₇H₂₄O₄
• CAS No.: 1410659-50-5
• Molecular Formula: C₁₇H₂₄O₄
• Molecular Weight: 292.375
• Mol file: 1410659-50-5.mol

Synonyms:C₁₇H₂₄O₄

Chemical Property of C₁₇H₂₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₄O₄

There total 6 articles about C₁₇H₂₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2-[(4S,6S)-6-(2-Benzyloxy-ethyl)-2,2-dimethyl-[1,3]dioxan-4-yl]-ethanol → C17H24O4 (1410659-50-5)

Guidance literature:

With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.07.043 DOI:10.1016/j.tetlet.2012.07.043

Reference yield:

C19H28O5 → C17H24O4 (1410659-50-5)

Guidance literature:

Multi-step reaction with 6 steps

1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / Inert atmosphere

2: toluene-4-sulfonic acid / methanol / Inert atmosphere

3: triethylamine / dichloromethane / Inert atmosphere

4: toluene-4-sulfonic acid / dichloromethane / Inert atmosphere

5: potassium carbonate / methanol / Inert atmosphere

6: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / Inert atmosphere

With sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1016/j.tetlet.2012.07.043 DOI:10.1016/j.tetlet.2012.07.043

Reference yield:

C19H28O4 (1410659-57-2) → C17H24O4 (1410659-50-5)

Guidance literature:

Multi-step reaction with 7 steps

1: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane / -20 °C / Inert atmosphere

2: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / Inert atmosphere

3: toluene-4-sulfonic acid / methanol / Inert atmosphere

4: triethylamine / dichloromethane / Inert atmosphere

5: toluene-4-sulfonic acid / dichloromethane / Inert atmosphere

6: potassium carbonate / methanol / Inert atmosphere

7: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / Inert atmosphere

With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; dichloromethane; 1: |Sharpless Asymmetric Epoxidation;

DOI:10.1016/j.tetlet.2012.07.043 DOI:10.1016/j.tetlet.2012.07.043

upstream raw materials:

C₁₉H₂₈O₄

C₁₉H₃₀O₅

C₁₄H₂₂O₄

C₁₆H₂₄O₅

Downstream raw materials:

C₁₉H₃₀O₆

C₂₂H₃₄O₆

C₂₂H₃₄O₆

C₂₂H₃₄O₆