Technology Process of N,N-diisopropyl-3-(2-benzyloxy-5-methyl-phenyl)-3-phenyl-propane amide
There total 4 articles about N,N-diisopropyl-3-(2-benzyloxy-5-methyl-phenyl)-3-phenyl-propane amide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-(2-benzyloxy-5-methyl-phenyl)-3-phenyl propionic acid; diisopropylamine;
In
toluene;
at 0 - 10 ℃;
With
isopropyl alcohol;
at 50 - 60 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide; water / methanol / Inert atmosphere; Reflux
1.2: pH 1 - 2
2.1: toluene / 0 - 10 °C
2.2: 50 - 60 °C
With
water; potassium hydroxide;
In
methanol; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sulfuric acid / 120 - 125 °C / Inert atmosphere
2.1: potassium carbonate / acetone / Reflux
3.1: potassium hydroxide; water / methanol / Inert atmosphere; Reflux
3.2: pH 1 - 2
4.1: toluene / 0 - 10 °C
4.2: 50 - 60 °C
With
sulfuric acid; water; potassium carbonate; potassium hydroxide;
In
methanol; acetone; toluene;
