16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-17-oxo-5-androsten-3β-yl acetate

Base Information

Chemical Name:16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-17-oxo-5-androsten-3β-yl acetate
CAS No.:929683-37-4
Molecular Formula:C₃₅H₄₄N₂O₅
Molecular Weight:572.745
Hs Code.:

Synonyms:16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-17-oxo-5-androsten-3β-yl acetate

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Chemical Property of 16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-17-oxo-5-androsten-3β-yl acetate

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Technology Process of 16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-17-oxo-5-androsten-3β-yl acetate

There total 3 articles about 16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-17-oxo-5-androsten-3β-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.04%

: 929683-36-3
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxy-benzylidene]-17-oxo-5-androsten-3β-ol

: 108-24-7
acetic anhydride

: 929683-37-4
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-17-oxo-5-androsten-3β-yl acetate

Guidance literature:: With pyridine; for 2h; Heating / reflux;

Reference yield:

: 151719-92-5
3-methoxy-4-(3-chloropropoxy) benzaldehyde

: 929683-37-4
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-17-oxo-5-androsten-3β-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol / 2 h / 20 °C

2: 5 h / 110 - 120 °C

3: pyridine / 2 h

With pyridine; sodium hydroxide; In methanol;

Reference yield:

: 53-43-0
dehydroepiandrosterone

: 929683-37-4
16-[4-{3-(imidazol-1-yl)propoxy}-3-methoxybenzylidene]-17-oxo-5-androsten-3β-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol / 2 h / 20 °C

2: 5 h / 110 - 120 °C

3: pyridine / 2 h

With pyridine; sodium hydroxide; In methanol;