Technology Process of C33H43N3O6
There total 9 articles about C33H43N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 2.08333h;
DOI:10.1039/c3ob41338a
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: triethylamine / 3 h / 20 °C
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.08 h / -78 °C
2.2: 0.17 h / 0 °C
3.1: palladium on activated charcoal; hydrogen / methanol / 15 h
4.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 18 h / 0 - 20 °C
5.1: triethylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 1.33 h / 0 - 20 °C
6.1: trifluoroacetic acid / dichloromethane / -5 °C
7.1: triethylamine / dichloromethane / 0.5 h / 0 °C
8.1: triethylamine / dichloromethane / 2.08 h / 0 - 20 °C
With
lithium hydroxide monohydrate; palladium on activated charcoal; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; triethylamine; trifluoroacetic acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c3ob41338a
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.08 h / -78 °C
1.2: 0.17 h / 0 °C
2.1: palladium on activated charcoal; hydrogen / methanol / 15 h
3.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 18 h / 0 - 20 °C
4.1: triethylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 1.33 h / 0 - 20 °C
5.1: trifluoroacetic acid / dichloromethane / -5 °C
6.1: triethylamine / dichloromethane / 0.5 h / 0 °C
7.1: triethylamine / dichloromethane / 2.08 h / 0 - 20 °C
With
lithium hydroxide monohydrate; palladium on activated charcoal; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; triethylamine; trifluoroacetic acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c3ob41338a