1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-ol

Base Information

• Chemical Name: 1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-ol
• CAS No.: 1064688-50-1
• Molecular Formula: C₁₆H₂₀ClFOS
• Molecular Weight: 314.852

Synonyms:1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-ol

Chemical Property of 1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-ol

Chemical Property:

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Technology Process of 1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-ol

There total 1 articles about 1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

6-[(2-chloro-4-fluorobenzyl)sulfanyl]-1-cyclohexene-1-carbaldehyde (1064687-61-1) + ethylmagnesium bromide (925-90-6) → 1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-ol (1064688-50-1)

Guidance literature:

In tetrahydrofuran; diethyl ether; for 1.5h;

DOI:10.1016/j.bmc.2008.01.030

Reference yield: 54.0%

1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-ol (1064688-50-1) → 1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-one (1028450-37-4)

Guidance literature:

With tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In dichloromethane; at 0 ℃; for 1h;

DOI:10.1016/j.bmc.2008.01.030

Reference yield: 36.0%

1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-ol (1064688-50-1) → C16H20ClFO3S (1028449-95-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In ethyl acetate;

DOI:10.1016/j.bmc.2008.01.030

upstream raw materials:

6-[(2-chloro-4-fluorobenzyl)sulfanyl]-1-cyclohexene-1-carbaldehyde

ethylmagnesium bromide

Downstream raw materials:

1-{6-[(2-chloro-4-fluorobenzyl)sulfanyl]cyclohex-1-en-1-yl}propan-1-one

C₁₆H₂₀ClFO₃S

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