phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2,4-dideoxy-α-D-lyxo-hexopyranoside

Base Information

Chemical Name:phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2,4-dideoxy-α-D-lyxo-hexopyranoside
CAS No.:161614-93-3
Molecular Formula:C₂₉H₂₉NO₇
Molecular Weight:503.552
Hs Code.:

Synonyms:phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2,4-dideoxy-α-D-lyxo-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2,4-dideoxy-α-D-lyxo-hexopyranoside

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Technology Process of phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2,4-dideoxy-α-D-lyxo-hexopyranoside

There total 5 articles about phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2,4-dideoxy-α-D-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 161614-92-2
phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-4-O-((1-imidazolido)-thiocarbonyl)-α-D-mannopyranoside

: 161614-93-3
phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2,4-dideoxy-α-D-lyxo-hexopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 0.833333h; Heating;
DOI:10.1016/S0957-4166(00)80390-0

Reference yield:

: 10375-65-2
phenylmethyl 3,4,6-tri-O-acetyl-2-acetylamino-2-deoxy-α-D-mannopyranoside

: 161614-93-3
phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2,4-dideoxy-α-D-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / NaOMe / methanol / 5 h

2: 47 percent / pyridine / CH₂Cl₂ / 24 h

3: 85 percent / CH₂Cl₂ / 24 h / Ambient temperature

4: 80 percent / Bu₃SnH, AIBN / toluene / 0.83 h / Heating

With pyridine; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium methylate; In methanol; dichloromethane; toluene;
DOI:10.1016/S0957-4166(00)80390-0

Reference yield:

: 3006-60-8,4539-83-7,6730-10-5,7772-79-4,7784-54-5,10385-50-9,14086-90-9,26151-16-6,76375-60-5,95341-98-3,95341-99-4,134451-91-5,134451-96-0,136982-81-5,145375-11-7,148347-15-3,76375-61-6
1,3,4,6-tetra-O-acetyl-2-acetamido-2-deoxy-α,β-D-mannopyranose

: 161614-93-3
phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2,4-dideoxy-α-D-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 63 percent / BF₃*Et₂O / nitromethane / 1 h / 80 °C

2: 100 percent / NaOMe / methanol / 5 h

3: 47 percent / pyridine / CH₂Cl₂ / 24 h

4: 85 percent / CH₂Cl₂ / 24 h / Ambient temperature

5: 80 percent / Bu₃SnH, AIBN / toluene / 0.83 h / Heating

With pyridine; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; sodium methylate; In methanol; nitromethane; dichloromethane; toluene;
DOI:10.1016/S0957-4166(00)80390-0