1,4-bis-2-(2'-ethylhexyloxy)benzene

Base Information

Chemical Name:1,4-bis-2-(2'-ethylhexyloxy)benzene
CAS No.:248587-90-8
Molecular Formula:C₂₂H₃₄O₃S₄
Molecular Weight:474.774
Hs Code.:

1,4-bis<ethoxy(thiocarbonyl)thiomethyl>-2-(2'-ethylhexyloxy)benzene

Synonyms:1,4-bis-2-(2'-ethylhexyloxy)benzene

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Chemical Property of 1,4-bis-2-(2'-ethylhexyloxy)benzene

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Technology Process of 1,4-bis-2-(2'-ethylhexyloxy)benzene

There total 4 articles about 1,4-bis-2-(2'-ethylhexyloxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 140-89-6
potassium ethyl xanthogenate

: 161960-53-8
1,4-bis(bromomethyl)-2-(2'-ethylhexyloxy)benzene

: 248587-90-8
1,4-bis-2-(2'-ethylhexyloxy)benzene

Guidance literature:: With tetrabutylammomium bromide; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1039/a902602i

Reference yield:

: 166447-07-0
2-(2'-ethylhexyloxy)-p-xylene

: 248587-90-8
1,4-bis-2-(2'-ethylhexyloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: NBS; AIBN / CCl₄ / 4 h / Heating

2: 98 percent / (n-Bu)4NBr / CH₂Cl₂ / 4 h / 20 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; In tetrachloromethane; dichloromethane; 1: Bromination / 2: Alkylation;
DOI:10.1039/a902602i

Reference yield:

: 248587-84-0
1,4-bis(hydroxymethyl)-2-(2'-ethylhexyloxy)benzene

: 248587-90-8
1,4-bis-2-(2'-ethylhexyloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / PBr₃ / CH₂Cl₂ / 18 h / 20 °C

2: 98 percent / (n-Bu)4NBr / CH₂Cl₂ / 4 h / 20 °C

With tetrabutylammomium bromide; phosphorus tribromide; In dichloromethane; 1: Bromination / 2: Alkylation;
DOI:10.1039/a902602i