4,5-di-O-benzyl-6-methyl-L-galacto-(2S)-methoxy-1,2λ⁵-oxaphosphorinan-2-one

Base Information

• Chemical Name: 4,5-di-O-benzyl-6-methyl-L-galacto-(2S)-methoxy-1,2λ⁵-oxaphosphorinan-2-one
• CAS No.: 266677-30-9
• Molecular Formula: C₂₀H₂₅O₆P
• Molecular Weight: 392.389

Synonyms:4,5-di-O-benzyl-6-methyl-L-galacto-(2S)-methoxy-1,2λ⁵-oxaphosphorinan-2-one

Chemical Property of 4,5-di-O-benzyl-6-methyl-L-galacto-(2S)-methoxy-1,2λ⁵-oxaphosphorinan-2-one

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Technology Process of 4,5-di-O-benzyl-6-methyl-L-galacto-(2S)-methoxy-1,2λ⁵-oxaphosphorinan-2-one

There total 1 articles about 4,5-di-O-benzyl-6-methyl-L-galacto-(2S)-methoxy-1,2λ⁵-oxaphosphorinan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-di-O-benzyl-5-deoxy-1-dimethylphosphonyl-4-O-formyl-L-fucose (266677-27-4) → 4,5-di-O-benzyl-6-methyl-L-galacto-(2S)-methoxy-1,2λ5-oxaphosphorinan-2-one (266677-30-9) + 4,5-di-O-benzyl-6-methyl-L-galacto-(2R)-methoxy-1,2λ5-oxaphosphorinan-2-one (266677-29-6)

Guidance literature:

With sodium methylate; In methanol; for 2h;

DOI:10.1021/jo991696l

Reference yield: 80.0%

4,5-di-O-benzyl-6-methyl-L-galacto-(2S)-methoxy-1,2λ5-oxaphosphorinan-2-one (266677-30-9) → 4,5-di-O-benzyl-6-methyl-L-galacto-(2R)-hydroxy-1,2λ5-oxaphosphorinan-2-one (266677-33-2)

Guidance literature:

With trimethylsilyl bromide; In dichloromethane; at 20 ℃;

DOI:10.1021/jo991696l

upstream raw materials:

2,3-di-O-benzyl-5-deoxy-1-dimethylphosphonyl-4-O-formyl-L-fucose

Downstream raw materials:

4,5-di-O-benzyl-6-methyl-L-galacto-(2R)-hydroxy-1,2λ⁵-oxaphosphorinan-2-one

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