6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diaminobenzene

Base Information

Chemical Name:6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diaminobenzene
CAS No.:1229608-46-1
Molecular Formula:C₂₅H₂₃N₂PS
Molecular Weight:414.511
Hs Code.:

Synonyms:6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diaminobenzene

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Chemical Property of 6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diaminobenzene

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Technology Process of 6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diaminobenzene

There total 2 articles about 6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diaminobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1229608-45-0
4-(2-(diphenylphosphinothioyl)phenyl)-7-methyl-2,1,3-benzothiadiazole

: 1229608-46-1
6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diaminobenzene

Guidance literature:: With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; In ethanol; for 1h; Inert atmosphere; Reflux;
DOI:10.1021/ja102428q

Reference yield:

: 1134641-48-7
C₂₅H₁₉N₂OPS

: 1229608-46-1
6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diaminobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorosilane; triethylamine / toluene / 0 - 100 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate; cobalt(II) chloride hexahydrate / ethanol / 1 h / Inert atmosphere; Reflux

With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; trichlorosilane; triethylamine; In ethanol; toluene;
DOI:10.1002/anie.201103792

Reference yield: 79.0%

: 1229608-46-1
6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diaminobenzene

: 2258-42-6
formyl acetic anhydride

: 1229608-40-5
6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diisocyanobenzene

Guidance literature:: 6-methyl-3-(2-(diphenylphosphinothioyl)phenyl)-1,2-diaminobenzene; formyl acetic anhydride; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

With triethylamine; trichlorophosphate; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/anie.201103792