ethyl 2-diazo-3-(N-(2,4-dimethoxybenzyl)-N-(phenyl)amino)-3-oxopropanoate

Base Information

Chemical Name:ethyl 2-diazo-3-(N-(2,4-dimethoxybenzyl)-N-(phenyl)amino)-3-oxopropanoate
CAS No.:1193723-64-6
Molecular Formula:C₂₀H₂₁N₃O₅
Molecular Weight:383.404
Hs Code.:

Synonyms:ethyl 2-diazo-3-(N-(2,4-dimethoxybenzyl)-N-(phenyl)amino)-3-oxopropanoate

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Chemical Property of ethyl 2-diazo-3-(N-(2,4-dimethoxybenzyl)-N-(phenyl)amino)-3-oxopropanoate

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Technology Process of ethyl 2-diazo-3-(N-(2,4-dimethoxybenzyl)-N-(phenyl)amino)-3-oxopropanoate

There total 1 articles about ethyl 2-diazo-3-(N-(2,4-dimethoxybenzyl)-N-(phenyl)amino)-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 57072-87-4
chlorocarbonyl-diazo-acetic acid ethyl ester

: 356094-10-5
N-{[2,4-bis(methyloxy)phenyl]methyl}aniline

: 1193723-64-6
ethyl 2-diazo-3-(N-(2,4-dimethoxybenzyl)-N-(phenyl)amino)-3-oxopropanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.08.006

Reference yield: 78.0%

: 1193723-64-6
ethyl 2-diazo-3-(N-(2,4-dimethoxybenzyl)-N-(phenyl)amino)-3-oxopropanoate

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1193723-78-2
ethyl 1-N-(2,4-dimethoxybenzyl)-2-(triisopropylsilyloxy)-1H-indole-3-carboxylate

Guidance literature:: ethyl 2-diazo-3-(N-(2,4-dimethoxybenzyl)-N-(phenyl)amino)-3-oxopropanoate; With tetrakis(μ-trifluoroacetamidato)dirhodium(II); In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

triisopropylsilyl trifluoromethanesulfonate; With triethylamine; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;
DOI:10.1016/j.tet.2009.08.006