exo-3-(methoxycarbonyl)-endo-3-carboxy-N-phenyl-6,7-diazatricyclo<3.2.20^2,4>non-8-ene-6,7-dicarboximide

Base Information

• Chemical Name: exo-3-(methoxycarbonyl)-endo-3-carboxy-N-phenyl-6,7-diazatricyclo<3.2.20^2,4>non-8-ene-6,7-dicarboximide
• CAS No.: 109746-66-9
• Molecular Formula: C₁₈H₁₅N₃O₆
• Molecular Weight: 369.334

Synonyms:exo-3-(methoxycarbonyl)-endo-3-carboxy-N-phenyl-6,7-diazatricyclo<3.2.20^2,4>non-8-ene-6,7-dicarboximide

Chemical Property of exo-3-(methoxycarbonyl)-endo-3-carboxy-N-phenyl-6,7-diazatricyclo<3.2.20^2,4>non-8-ene-6,7-dicarboximide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of exo-3-(methoxycarbonyl)-endo-3-carboxy-N-phenyl-6,7-diazatricyclo<3.2.20^2,4>non-8-ene-6,7-dicarboximide

There total 1 articles about exo-3-(methoxycarbonyl)-endo-3-carboxy-N-phenyl-6,7-diazatricyclo<3.2.20^2,4>non-8-ene-6,7-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Phenylurazole (15988-11-1) + 7-(methoxycarbonyl)cycloheptatriene (32399-46-5) → exo-3-(methoxycarbonyl)-endo-3-carboxy-N-phenyl-6,7-diazatricyclo<3.2.202,4>non-8-ene-6,7-dicarboximide (109746-66-9)

Guidance literature:

With lithium diisopropyl amide; Yield given. Multistep reaction; 1) THF, -78 deg C, 30 min, 2) THF, 20 deg C, 30 min;

Reference yield: 88.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + exo-3-(methoxycarbonyl)-endo-3-carboxy-N-phenyl-6,7-diazatricyclo<3.2.202,4>non-8-ene-6,7-dicarboximide (109746-66-9) → 3,3-dicarboxy-N-phenyl-6,7-diazatricyclo<3.2.2.02,4>non-8-ene-6,7-dicarboximide (109764-59-2)

Guidance literature:

In diethyl ether; for 0.25h;

Reference yield: 65.0%

exo-3-(methoxycarbonyl)-endo-3-carboxy-N-phenyl-6,7-diazatricyclo<3.2.202,4>non-8-ene-6,7-dicarboximide (109746-66-9) → C17H15N3O4 (65138-04-7)

Guidance literature:

With copper(I) oxide; In N,N-dimethyl-formamide; toluene; at 130 ℃; for 2h;

upstream raw materials:

4-Phenylurazole

7-(methoxycarbonyl)cycloheptatriene

Downstream raw materials:

3,3-dicarboxy-N-phenyl-6,7-diazatricyclo<3.2.2.0^2,4>non-8-ene-6,7-dicarboximide

C₁₇H₁₅N₃O₄

methyl (1R*,7S*,8R*,9S*,10S*)-2-methyl-3,5-dioxo-4-phenyl-2,4,6-triazatetracyclo<5.3.2.0^1.6.0^8,10>dodec-11-ene-9-carboxylate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 109746-66-9 exo-3-(methoxycarbonyl)-endo-3-carboxy-N-phenyl-6,7-diazatricyclo<3.2.20^2,4>non-8-ene-6,7-dicarboximide

Send

Send

Metric Ton KG G Pound L ML

Send

Send