(4-bromo-2-(propan-2-ylideneaminooxy)phenyl)(2-(diethoxymethyl)phenyl)methanone

Base Information

Chemical Name:(4-bromo-2-(propan-2-ylideneaminooxy)phenyl)(2-(diethoxymethyl)phenyl)methanone
CAS No.:1261604-01-6
Molecular Formula:C₂₁H₂₄BrNO₄
Molecular Weight:434.33
Hs Code.:

Synonyms:(4-bromo-2-(propan-2-ylideneaminooxy)phenyl)(2-(diethoxymethyl)phenyl)methanone

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Chemical Property of (4-bromo-2-(propan-2-ylideneaminooxy)phenyl)(2-(diethoxymethyl)phenyl)methanone

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Technology Process of (4-bromo-2-(propan-2-ylideneaminooxy)phenyl)(2-(diethoxymethyl)phenyl)methanone

There total 4 articles about (4-bromo-2-(propan-2-ylideneaminooxy)phenyl)(2-(diethoxymethyl)phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1261603-99-9
(4-bromo-2-fluorophenyl)(2-(diethoxymethyl)phenyl)methanone

: 127-06-0
acetone oxime

: 1261604-01-6
(4-bromo-2-(propan-2-ylideneaminooxy)phenyl)(2-(diethoxymethyl)phenyl)methanone

Guidance literature:: acetone oxime; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.333333h; Inert atmosphere;

(4-bromo-2-fluorophenyl)(2-(diethoxymethyl)phenyl)methanone; In tetrahydrofuran; at 20 ℃; for 6.33333h; Inert atmosphere; Reflux;

Reference yield:

: 57848-46-1
4-bromo-2-fluorobenzaldehyde

: 1261604-01-6
(4-bromo-2-(propan-2-ylideneaminooxy)phenyl)(2-(diethoxymethyl)phenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: hexane; diethyl ether / 1.25 h / -70 - -60 °C / Inert atmosphere

1.2: 4 h / -60 - 10 °C

2.1: sodium hydrogencarbonate; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; tert-butyl alcohol / 20 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

3.2: 6.33 h / 20 °C / Inert atmosphere; Reflux

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; potassium tert-butylate; sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; hexane; water; tert-butyl alcohol;

Reference yield:

: 35822-58-3
2-bromobenzaldehyde diethyl acetal

: 1261604-01-6
(4-bromo-2-(propan-2-ylideneaminooxy)phenyl)(2-(diethoxymethyl)phenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: hexane; diethyl ether / 1.25 h / -70 - -60 °C / Inert atmosphere

1.2: 4 h / -60 - 10 °C

2.1: sodium hydrogencarbonate; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; tert-butyl alcohol / 20 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

3.2: 6.33 h / 20 °C / Inert atmosphere; Reflux

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; potassium tert-butylate; sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; hexane; water; tert-butyl alcohol;