C₃₉H₄₀FN₇O₃

Base Information

• Chemical Name: C₃₉H₄₀FN₇O₃
• CAS No.: 1383121-92-3
• Molecular Formula: C₃₉H₄₀FN₇O₃
• Molecular Weight: 673.79
• Mol file: 1383121-92-3.mol

Synonyms:C₃₉H₄₀FN₇O₃

Chemical Property of C₃₉H₄₀FN₇O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₉H₄₀FN₇O₃

There total 9 articles about C₃₉H₄₀FN₇O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C48H50FN7O5S (1383122-88-0) → C39H40FN7O3 (1383121-92-3)

Guidance literature:

With trimethylsilyl bromide; methyl-phenyl-thioether; ethane-1,2-dithiol; 3-methyl-phenol; trifluoroacetic acid; at 0 - 20 ℃; for 3.5h; Inert atmosphere;

DOI:10.1016/j.bmcl.2012.04.032

Reference yield:

C18H22N2O2 (1383122-36-8) → C39H40FN7O3 (1383121-92-3)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium tris(acetoxy)borohydride / dichloromethane

2: trifluoroacetic acid

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 43 h / 0 - 20 °C

4: trimethylsilyl bromide; methyl-phenyl-thioether; ethane-1,2-dithiol; 3-methyl-phenol; trifluoroacetic acid / 3.5 h / 0 - 20 °C / Inert atmosphere

With trimethylsilyl bromide; methyl-phenyl-thioether; sodium tris(acetoxy)borohydride; ethane-1,2-dithiol; 3-methyl-phenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2012.04.032

Reference yield:

C25H25FN2O3 (1383122-48-2) → C39H40FN7O3 (1383121-92-3)

Guidance literature:

Multi-step reaction with 3 steps

1: trifluoroacetic acid

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 43 h / 0 - 20 °C

3: trimethylsilyl bromide; methyl-phenyl-thioether; ethane-1,2-dithiol; 3-methyl-phenol; trifluoroacetic acid / 3.5 h / 0 - 20 °C / Inert atmosphere

With trimethylsilyl bromide; methyl-phenyl-thioether; ethane-1,2-dithiol; 3-methyl-phenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2012.04.032

upstream raw materials:

C₄₈H₅₀FN₇O₅S

C₃₂H₄₃N₅O₅S

4-[(2-nitro-benzenesulfonylamino)-methyl]-benzoic acid tert-butyl ester

C₁₈H₂₂N₂O₂