(S)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane

Base Information

Chemical Name:(S)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane
CAS No.:1427549-19-6
Molecular Formula:C₂₀H₂₉BO₂
Molecular Weight:312.26
Hs Code.:

Synonyms:(S)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane

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Technology Process of (S)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane

There total 1 articles about (S)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₈B₂O₄

: 639005-99-5
(E)-(5-chloropent-3-en-1-yl)benzene

: 1427549-19-6
(S)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane

: (R)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane

Guidance literature:: With (R,R)-(?)-2,3-bis(t-butylmethylphosphino)quinoxaline; bis(η3-allyl-μ-chloropalladium(II)); cesium fluoride; In tetrahydrofuran; water; at 60 ℃; for 16h; Overall yield = 75 %; Overall yield = 65 mg; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol400088g

Reference yield:

: 1427549-19-6
(S)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane

: 1427549-51-6
C₁₄H₁₈O

Guidance literature:: With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; at 0 - 23 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol400088g

Reference yield:

: 1427549-19-6
(S)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane

: (S)-(3-vinyl-5-hexen-1-yl)benzene

Guidance literature:: (S)-4,4,5,5-tetramethyl-2-(4-phenethylhexa-1,5-dien-2-yl)-1,3,2-dioxaborolane; With copper(ll) bromide; In methanol; water; at 90 ℃; for 12h; Inert atmosphere;

With n-butyllithium; water; Inert atmosphere;
DOI:10.1021/ol400088g