Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)][BF₄]

Base Information

• Chemical Name: Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)][BF₄]
• CAS No.: 66609-55-0
• Molecular Formula: BF₄*C₄₀H₃₆O₂P₂Rh
• Molecular Weight: 800.382

Synonyms:Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)][BF₄]

Chemical Property of Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)][BF₄]

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Technology Process of Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)][BF₄]

There total 3 articles about Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)][BF₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrafluoroboric acid + carbonyl(diphenyltriazene)bis(triphenylphosphine)rhodium tetrafluoroborate (66540-42-9) → Rh(CO)(P(C6H5)3)2(OC(CH3)2)(1+)*BF4(1-)=[Rh(CO)(P(C6H5)3)2(OC(CH3)2)][BF4] (66609-55-0)

Guidance literature:

In ethanol; water; N2-atmosphere; addn. of aq. HBF4 to soln. of Rh-complex in EtOH; recrystn. (Me2CO/Et2O);

DOI:10.1039/DT9780000050

Reference yield:

tetrafluoroboric acid + Rh(CO)(P(C6H5)3)2((CH3C6H4)2N3H)(1+)*BF4(1-)=[Rh(CO)(P(C6H5)3)2((CH3C6H4)2N3H)][BF4] (66540-44-1) → Rh(CO)(P(C6H5)3)2(OC(CH3)2)(1+)*BF4(1-)=[Rh(CO)(P(C6H5)3)2(OC(CH3)2)][BF4] (66609-55-0)

Guidance literature:

In ethanol; water; N2-atmosphere; addn. of aq. HBF4 to soln. of Rh-complex in EtOH; recrystn. (Me2CO/Et2O);

DOI:10.1039/DT9780000050

Reference yield:

tetrafluoroboric acid + Rh(CO)(P(C6H5)3)2((FC6H4)2N3H)(1+)*BF4(1-)=[Rh(CO)(P(C6H5)3)2((FC6H4)2N3H)][BF4] (66540-46-3) → Rh(CO)(P(C6H5)3)2(OC(CH3)2)(1+)*BF4(1-)=[Rh(CO)(P(C6H5)3)2(OC(CH3)2)][BF4] (66609-55-0)

Guidance literature:

In ethanol; water; N2-atmosphere; addn. of aq. HBF4 to soln. of Rh-complex in EtOH; recrystn. (Me2CO/Et2O);

DOI:10.1039/DT9780000050

upstream raw materials:

carbonyl(diphenyltriazene)bis(triphenylphosphine)rhodium tetrafluoroborate

Rh(CO)(P(C₆H₅)3)2((CH₃C₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((CH₃C₆H₄)2N₃H)][BF₄]

Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)][BF₄]

Downstream raw materials:

Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)][BF₄]

Rh(CO)(P(C₆H₅)3)2((CH₃C₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((CH₃C₆H₄)2N₃H)][BF₄]

chlorocarbonylbis(triphenylphosphine)rhodium(I)

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