Technology Process of C59H63N7O11Si
There total 5 articles about C59H63N7O11Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate;
In
dichloromethane; water;
at 20 ℃;
for 3h;
DOI:10.1021/jo400651k
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic anhydride / acetic acid / 72 h / 20 °C
2.1: bromine / acetonitrile / 0.5 h / 0 °C
2.2: 2.17 h / 0 - 60 °C
3.1: potassium carbonate / methanol / 12 h / 20 °C
4.1: pyridine / 12 h / 20 °C
5.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 3 h / 20 °C
With
copper(ll) sulfate pentahydrate; bromine; acetic anhydride; potassium carbonate; sodium L-ascorbate;
In
pyridine; methanol; dichloromethane; water; acetic acid; acetonitrile;
1.1: |Pummerer Sulfoxide Rearrangement;
DOI:10.1021/jo400651k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / methanol / 12 h / 20 °C
2: pyridine / 12 h / 20 °C
3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 3 h / 20 °C
With
copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate;
In
pyridine; methanol; dichloromethane; water;
DOI:10.1021/jo400651k