(+/-)-tert-butyl threo-3-<(benzyloxycarbonyl)oxy>-2-fluorotetradecanoate

Base Information

Chemical Name:(+/-)-tert-butyl threo-3-<(benzyloxycarbonyl)oxy>-2-fluorotetradecanoate
CAS No.:120927-33-5
Molecular Formula:C₂₆H₄₁FO₅
Molecular Weight:452.607
Hs Code.:

Synonyms:(+/-)-tert-butyl threo-3-<(benzyloxycarbonyl)oxy>-2-fluorotetradecanoate

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Chemical Property of (+/-)-tert-butyl threo-3-<(benzyloxycarbonyl)oxy>-2-fluorotetradecanoate

Chemical Property:

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Technology Process of (+/-)-tert-butyl threo-3-<(benzyloxycarbonyl)oxy>-2-fluorotetradecanoate

There total 3 articles about (+/-)-tert-butyl threo-3-<(benzyloxycarbonyl)oxy>-2-fluorotetradecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120927-31-3
(+/-)-tert-butyl threo-2-fluoro-3-hydroxytetradecanoate

: 501-53-1,94274-21-2
benzyl chloroformate

: 120927-33-5
(+/-)-tert-butyl threo-3-<(benzyloxycarbonyl)oxy>-2-fluorotetradecanoate

Guidance literature:: With dmap; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo00276a050

Reference yield:

: 112-54-9
Dodecanal

: 120927-33-5
(+/-)-tert-butyl threo-3-<(benzyloxycarbonyl)oxy>-2-fluorotetradecanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) hexamethyldisilazane, butyllithium / 1.) THF, hexane, -78 deg C, 5 min, 2.) -78 deg C, 20 min

2: 57 percent / magnesium monoperphthalate hexahydrate / ethanol / 18 h / 50 °C

3: DMAP / CH₂Cl₂ / 1 h / 0 °C

With dmap; n-butyllithium; magnesium monoperoxyphthalate hexahydrate; 1,1,1,3,3,3-hexamethyl-disilazane; In ethanol; dichloromethane;
DOI:10.1021/jo00276a050

Reference yield:

: 120927-30-2
(+/-)-threo-2,2-dimethyl-4-fluoro-5-hydroxy-3-hexadecanone

: 120927-33-5
(+/-)-tert-butyl threo-3-<(benzyloxycarbonyl)oxy>-2-fluorotetradecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / magnesium monoperphthalate hexahydrate / ethanol / 18 h / 50 °C

2: DMAP / CH₂Cl₂ / 1 h / 0 °C

With dmap; magnesium monoperoxyphthalate hexahydrate; In ethanol; dichloromethane;
DOI:10.1021/jo00276a050