Technology Process of C18H20Cl2O2
There total 4 articles about C18H20Cl2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrachloromethane; triphenylphosphine;
Reflux;
DOI:10.1021/jm7010707
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / 24 h / 50 °C / Inert atmosphere; Schlenk technique
2: sodium tetrahydroborate / tetrahydrofuran; ethanol / 10 h / Cooling with ice; Reflux; Inert atmosphere; Schlenk technique
3: thionyl chloride / chloroform / 12 h / Inert atmosphere; Schlenk technique; Reflux
With
sodium tetrahydroborate; thionyl chloride; potassium carbonate;
In
tetrahydrofuran; ethanol; chloroform;
DOI:10.1039/c4ce01519c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 10 h / Cooling with ice; Reflux; Inert atmosphere; Schlenk technique
2: thionyl chloride / chloroform / 12 h / Inert atmosphere; Schlenk technique; Reflux
With
sodium tetrahydroborate; thionyl chloride;
In
tetrahydrofuran; ethanol; chloroform;
DOI:10.1039/c4ce01519c