Methyl (+/-)-3-carbomethoxy-4-[2-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-methoxyphenyl]butanoate

Base Information

Chemical Name:Methyl (+/-)-3-carbomethoxy-4-[2-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-methoxyphenyl]butanoate
CAS No.:205676-68-2
Molecular Formula:C₂₁H₃₁NO₇
Molecular Weight:409.48
Hs Code.:

Synonyms:Methyl (+/-)-3-carbomethoxy-4-[2-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-methoxyphenyl]butanoate

Suppliers and Price of Methyl (+/-)-3-carbomethoxy-4-[2-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-methoxyphenyl]butanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methyl (+/-)-3-carbomethoxy-4-[2-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-methoxyphenyl]butanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methyl (+/-)-3-carbomethoxy-4-[2-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-methoxyphenyl]butanoate

There total 5 articles about Methyl (+/-)-3-carbomethoxy-4-[2-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-methoxyphenyl]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₉NO₇

: 205676-68-2
Methyl (+/-)-3-carbomethoxy-4-[2-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-methoxyphenyl]butanoate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; for 5h; under 2585.81 Torr;

Reference yield:

: 205676-67-1
3-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-bromoanisole

: 6163-58-2
tris-(o-tolyl)phosphine

: 205676-68-2
Methyl (+/-)-3-carbomethoxy-4-[2-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-methoxyphenyl]butanoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; palladium diacetate; In ethyl acetate; propiononitrile;

Reference yield:

: 19614-12-1
2-bromo-5-methoxybenzyl bromide

: 205676-68-2
Methyl (+/-)-3-carbomethoxy-4-[2-[N-(tert-butoxycarbonyl)-N-methylamino]methyl-4-methoxyphenyl]butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran; water / 2.5 h / 20 °C

2: chloroform / 0.75 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / palladium diacetate; tris-(o-tolyl)phosphine / propiononitrile / 0.75 h / Heating / reflux

4: hydrogen / palladium 10% on activated carbon / methanol / 5 h / 2585.81 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium diacetate; palladium 10% on activated carbon; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; chloroform; water; propiononitrile;