sodium 3,5-dichloro-4-methoxybenzenesulfinate

Base Information

Chemical Name:sodium 3,5-dichloro-4-methoxybenzenesulfinate
CAS No.:125927-97-1
Molecular Formula:C₇H₅Cl₂O₃S*Na
Molecular Weight:263.077
Hs Code.:

Synonyms:sodium 3,5-dichloro-4-methoxybenzenesulfinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium 3,5-dichloro-4-methoxybenzenesulfinate

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Technology Process of sodium 3,5-dichloro-4-methoxybenzenesulfinate

There total 2 articles about sodium 3,5-dichloro-4-methoxybenzenesulfinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 35517-53-4
3,5-dichloro-4-methoxybenzenesulfonyl chloride

: 125927-97-1
sodium 3,5-dichloro-4-methoxybenzenesulfinate

Guidance literature:: With sodium hydrogencarbonate; sodium sulfite; In water; acetone; at 50 ℃; for 1h;
DOI:10.1021/jo00295a062

Reference yield:

: 13432-81-0
3,5-dichloro-4-hydroxybenzene-1-sulfonyl chloride

: 125927-97-1
sodium 3,5-dichloro-4-methoxybenzenesulfinate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / diethyl ether / 25 °C

2: 97 percent / Na₂SO₃, NaHCO₃ / H₂O; acetone / 1 h / 50 °C

With sodium hydrogencarbonate; sodium sulfite; In diethyl ether; water; acetone;
DOI:10.1021/jo00295a062