C₂₈H₂₄N₂O₄S

Base Information

Chemical Name:C₂₈H₂₄N₂O₄S
CAS No.:1423691-32-0
Molecular Formula:C₂₈H₂₄N₂O₄S
Molecular Weight:484.576
Hs Code.:

C<sub>28</sub>H<sub>24</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:C₂₈H₂₄N₂O₄S

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Chemical Property of C₂₈H₂₄N₂O₄S

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Technology Process of C₂₈H₂₄N₂O₄S

There total 8 articles about C₂₈H₂₄N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.7%

: 1423703-09-6
C₁₅H₁₂O₂

: 1423702-95-7
C₁₃H₁₃IN₂O₂S

: 1423691-32-0
C₂₈H₂₄N₂O₄S

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; triethylamine; for 2h; Inert atmosphere; Reflux;

Reference yield:

: 33626-98-1
methyl 6-bromo-2-naphthoate

: 1423691-32-0
C₂₈H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 8 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 - 20 °C

2: thionyl chloride; zinc(II) chloride / dichloromethane / -5 - 20 °C

3: acetonitrile / Reflux

4: acetic acid; water; sulfuric acid / 2 h / Reflux

5: hydrogenchloride / 2 h / Reflux

6: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / N,N-dimethyl-formamide / Inert atmosphere; Reflux

7: tetrabutyl ammonium fluoride / dichloromethane / 2 h / 20 °C

8: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / 2 h / Inert atmosphere; Reflux

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; lithium aluminium tetrahydride; thionyl chloride; sulfuric acid; tetrabutyl ammonium fluoride; water; acetic acid; triethylamine; zinc(II) chloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 32721-06-5
2-(6-bromonaphthalen-2-yl)acetic acid

: 1423691-32-0
C₂₈H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / 2 h / Reflux

2: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / N,N-dimethyl-formamide / Inert atmosphere; Reflux

3: tetrabutyl ammonium fluoride / dichloromethane / 2 h / 20 °C

4: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / 2 h / Inert atmosphere; Reflux

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;