3,5-O-(3,4-Dimethoxybenzylidene)-9,11-O-(2,4,6-trimethylbenzylidene)-(9S)-9-dihydroerythronolide A seco-acid methylester

Base Information

Chemical Name:3,5-O-(3,4-Dimethoxybenzylidene)-9,11-O-(2,4,6-trimethylbenzylidene)-(9S)-9-dihydroerythronolide A seco-acid methylester
CAS No.:131755-86-7
Molecular Formula:C₄₁H₆₂O₁₁
Molecular Weight:730.937
Hs Code.:

Synonyms:3,5-O-(3,4-Dimethoxybenzylidene)-9,11-O-(2,4,6-trimethylbenzylidene)-(9S)-9-dihydroerythronolide A seco-acid methylester

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Chemical Property of 3,5-O-(3,4-Dimethoxybenzylidene)-9,11-O-(2,4,6-trimethylbenzylidene)-(9S)-9-dihydroerythronolide A seco-acid methylester

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Technology Process of 3,5-O-(3,4-Dimethoxybenzylidene)-9,11-O-(2,4,6-trimethylbenzylidene)-(9S)-9-dihydroerythronolide A seco-acid methylester

There total 6 articles about 3,5-O-(3,4-Dimethoxybenzylidene)-9,11-O-(2,4,6-trimethylbenzylidene)-(9S)-9-dihydroerythronolide A seco-acid methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 131755-85-6
3,5-O-(3,4-Dimethoxybenzylidene)-13-O-(4-methoxybenzyl)-9,11-O-(2,4,6-trimethylbenzylidene)-(9S)-9-dihydroerythronolide A seco-acid methylester

: 131755-86-7
3,5-O-(3,4-Dimethoxybenzylidene)-9,11-O-(2,4,6-trimethylbenzylidene)-(9S)-9-dihydroerythronolide A seco-acid methylester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 0.333333h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85585-X

Reference yield:

: 131755-84-5
C₄₈H₆₈O₁₂

: 131755-86-7
3,5-O-(3,4-Dimethoxybenzylidene)-9,11-O-(2,4,6-trimethylbenzylidene)-(9S)-9-dihydroerythronolide A seco-acid methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / diethyl ether / 0.05 h / Ambient temperature

2: 80 percent / H₂ / 10percent Pd/C / ethanol / 0.33 h / Ambient temperature

With hydrogen; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1016/S0040-4020(01)85585-X

Reference yield:

: 131755-83-4
(2S,3R,4S,5R,6R,8R,9S,10S,11R,12R,13R)-3,5-(3,4-Dimethoxybenzylidenedioxy)-13-(4-methoxybenzyloxy)-2,4,6,8,10,12-hexamethyl-9,11-(2,4,6-trimethylbenzylidenedioxy)pentadecane-1,6,12-triol

: 131755-86-7
3,5-O-(3,4-Dimethoxybenzylidene)-9,11-O-(2,4,6-trimethylbenzylidene)-(9S)-9-dihydroerythronolide A seco-acid methylester

Guidance literature:: Multi-step reaction with 3 steps

1: 59.7 mg / Jones reagent / 1 h / -28 - -18 °C

2: 50 percent / diethyl ether / 0.05 h / Ambient temperature

3: 80 percent / H₂ / 10percent Pd/C / ethanol / 0.33 h / Ambient temperature

With jones reagent; hydrogen; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1016/S0040-4020(01)85585-X