Technology Process of C17H23N3O
There total 4 articles about C17H23N3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethanol;
for 5h;
under 2625.26 Torr;
DOI:10.1002/cmdc.201000244
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diethyl ether / 14 h / 20 °C
2: hydrogenchloride; acetic acid / water / 42 h / Reflux
3: palladium 10% on activated carbon; hydrogen / ethanol / 5 h / 2625.26 Torr
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; acetic acid;
In
diethyl ether; ethanol; water;
1: Grignard reaction;
DOI:10.1002/cmdc.201000244
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C
1.2: 20 °C
2.1: diethyl ether / 14 h / 20 °C
3.1: hydrogenchloride; acetic acid / water / 42 h / Reflux
4.1: palladium 10% on activated carbon; hydrogen / ethanol / 5 h / 2625.26 Torr
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; sodium hydride; acetic acid;
In
diethyl ether; ethanol; water; N,N-dimethyl-formamide;
2.1: Grignard reaction;
DOI:10.1002/cmdc.201000244