Technology Process of hex-5-en-1-yn-3-ylcyclohexane
There total 2 articles about hex-5-en-1-yn-3-ylcyclohexane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; cesium fluoride;
In
tetrahydrofuran;
at 60 ℃;
for 14h;
Inert atmosphere;
sealed tube;
DOI:10.1021/ja302329f
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; cesium fluoride / tetrahydrofuran / 14 h / 60 °C / Inert atmosphere; sealed tube
With
dmap; tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; cesium fluoride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja302329f
