(2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-aminocyclopropanecarboxylate

Base Information

Chemical Name:(2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-aminocyclopropanecarboxylate
CAS No.:1071850-64-0
Molecular Formula:C₆₃H₈₀N₂O₁₂SSi
Molecular Weight:1117.49
Hs Code.:

(2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-aminocyclopropanecarboxylate

Synonyms:(2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-aminocyclopropanecarboxylate

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Chemical Property of (2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-aminocyclopropanecarboxylate

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Technology Process of (2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-aminocyclopropanecarboxylate

There total 1 articles about (2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-aminocyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1071850-62-8
(2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-azidocyclopropanecarboxylate

: 1071850-64-0
(2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-aminocyclopropanecarboxylate

Guidance literature:: With 1.3-propanedithiol; triethylamine; In methanol; at 23 ℃; for 15h; Inert atmosphere;
DOI:10.1002/anie.200802079

Reference yield: 78.0%

: 1071850-64-0
(2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-aminocyclopropanecarboxylate

: 636-82-8
cyclohexene-1-carboxylic acid

: 1071850-66-2
(2E,5S,6S,7R,8Z)-11-[2-(tert-butoxycarbonyloxy)-5-methoxy-3-nitrophenyl]-6,8-dimethyl-11-(phenylsulfonyl)-7-(triisopropylsiloxy)-1-(triphenylmethoxy)undeca-2,8-dien-5-yl 1-(cyclohex-1-enecarboxamido)cyclopropanecarboxylate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 23 ℃; for 21h; Inert atmosphere;
DOI:10.1002/anie.200802079