<(2,4-Dimethoxyphenyl)carbamoyl>phenyl-thiocarbamidsaeure-O-methylester

Base Information

Chemical Name:<(2,4-Dimethoxyphenyl)carbamoyl>phenyl-thiocarbamidsaeure-O-methylester
CAS No.:73280-53-2
Molecular Formula:C₁₇H₁₈N₂O₄S
Molecular Weight:346.407
Hs Code.:

Synonyms:<(2,4-Dimethoxyphenyl)carbamoyl>phenyl-thiocarbamidsaeure-O-methylester

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Chemical Property of <(2,4-Dimethoxyphenyl)carbamoyl>phenyl-thiocarbamidsaeure-O-methylester

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Technology Process of <(2,4-Dimethoxyphenyl)carbamoyl>phenyl-thiocarbamidsaeure-O-methylester

There total 3 articles about <(2,4-Dimethoxyphenyl)carbamoyl>phenyl-thiocarbamidsaeure-O-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 73280-66-7
C₉H₈ClNO₂S

: 2735-04-8,161687-55-4
2,4-Dimethoxyaniline

: 73280-53-2
<(2,4-Dimethoxyphenyl)carbamoyl>phenyl-thiocarbamidsaeure-O-methylester

Guidance literature:: With triethylamine; In diethyl ether; at -20 ℃; for 1h;

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 73280-53-2
<(2,4-Dimethoxyphenyl)carbamoyl>phenyl-thiocarbamidsaeure-O-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: KOH (86percent)

2: diethyl ether / 2 h / -20 °C

3: 72 percent / Et₃N / diethyl ether / 1 h / -20 °C

With potassium hydroxide; triethylamine; In diethyl ether;

Reference yield:

: 73280-65-6
C₈H₈NOS^(1-)*K⁽¹⁺⁾

: 73280-53-2
<(2,4-Dimethoxyphenyl)carbamoyl>phenyl-thiocarbamidsaeure-O-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 2 h / -20 °C

2: 72 percent / Et₃N / diethyl ether / 1 h / -20 °C

With triethylamine; In diethyl ether;