3-<2-(3,4-dimethoxyphenyl)ethoxy>-2-hydroxy-3,3-diphenylpropionic acid methyl ester

Base Information

Chemical Name:3-<2-(3,4-dimethoxyphenyl)ethoxy>-2-hydroxy-3,3-diphenylpropionic acid methyl ester
CAS No.:204268-04-2
Molecular Formula:C₂₆H₂₈O₆
Molecular Weight:436.505
Hs Code.:

Synonyms:3-<2-(3,4-dimethoxyphenyl)ethoxy>-2-hydroxy-3,3-diphenylpropionic acid methyl ester

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Chemical Property of 3-<2-(3,4-dimethoxyphenyl)ethoxy>-2-hydroxy-3,3-diphenylpropionic acid methyl ester

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Technology Process of 3-<2-(3,4-dimethoxyphenyl)ethoxy>-2-hydroxy-3,3-diphenylpropionic acid methyl ester

There total 1 articles about 3-<2-(3,4-dimethoxyphenyl)ethoxy>-2-hydroxy-3,3-diphenylpropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 76527-25-8
3,3-diphenyloxirane-2-carboxylic acid methyl ester

: 7417-21-2
2-(3,4-dimethoxyphenyl)ethyl alcohol

: 204268-04-2
3-<2-(3,4-dimethoxyphenyl)ethoxy>-2-hydroxy-3,3-diphenylpropionic acid methyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jm9910425

Reference yield: 87.0%

: 204268-04-2
3-<2-(3,4-dimethoxyphenyl)ethoxy>-2-hydroxy-3,3-diphenylpropionic acid methyl ester

: 204268-05-3
3-<2-(3,4-dimethoxyphenyl)ethoxy>-2-hydroxy-3,3-diphenylpropionic acid

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; at 80 ℃; for 2h;
DOI:10.1021/jm9910425

Reference yield:

: 204268-04-2
3-<2-(3,4-dimethoxyphenyl)ethoxy>-2-hydroxy-3,3-diphenylpropionic acid methyl ester

: 204267-33-4
Lu 224332

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 1 N aq. NaOH / dioxane / 2 h / 80 °C

2: 64 g / LiNH₂ / dimethylformamide / 18 h / Ambient temperature

With sodium hydroxide; lithium amide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm9910425