1-Methoxy-4-[(2,2,2-trifluoro-ethoxy)-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-benzene

Base Information

• Chemical Name: 1-Methoxy-4-[(2,2,2-trifluoro-ethoxy)-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-benzene
• CAS No.: 150723-10-7
• Molecular Formula: C₁₂H₁₂F₆O₂S
• Molecular Weight: 334.282

Synonyms:1-Methoxy-4-[(2,2,2-trifluoro-ethoxy)-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-benzene

Chemical Property of 1-Methoxy-4-[(2,2,2-trifluoro-ethoxy)-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-benzene

Chemical Property:

Purity/Quality:

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Technology Process of 1-Methoxy-4-[(2,2,2-trifluoro-ethoxy)-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-benzene

There total 3 articles about 1-Methoxy-4-[(2,2,2-trifluoro-ethoxy)-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1-[Azido-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-4-methoxy-benzene (150723-08-3) → 1-Methoxy-4-[(2,2,2-trifluoro-ethoxy)-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-benzene (150723-10-7)

Guidance literature:

With NaCH₂CF₃; In various solvent(s); Ambient temperature;

Reference yield:

1-(diazidomethyl)-4-methoxybenzene (92567-07-2) → 1-Methoxy-4-[(2,2,2-trifluoro-ethoxy)-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-benzene (150723-10-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / dimethylsulfoxide; H₂O / 1 h / Ambient temperature

2: 89 percent / NaCH₂CF₃ / various solvent(s) / Ambient temperature

With NaCH₂CF₃; In water; dimethyl sulfoxide;

Reference yield:

2,2,2-trifluoroethoxide (24265-37-0) + C10H10F3OS(1+) (150723-12-9) → 1-Methoxy-4-[(2,2,2-trifluoro-ethoxy)-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-benzene (150723-10-7)

Guidance literature:

With sodium perchlorate; water; at 25 ℃; Equilibrium constant;

upstream raw materials:

2,2,2-trifluoroethoxide

C₁₀H₁₀F₃OS⁽¹⁺⁾

1-[Azido-(2,2,2-trifluoro-ethylsulfanyl)-methyl]-4-methoxy-benzene

1-(diazidomethyl)-4-methoxybenzene

Downstream raw materials:

C₁₀H₁₀F₃OS⁽¹⁺⁾

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