(S)-1-(1-hydroxy-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propan-2-yl)-3-isopropylurea

Base Information

Chemical Name:(S)-1-(1-hydroxy-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propan-2-yl)-3-isopropylurea
CAS No.:1417653-80-5
Molecular Formula:C₁₉H₂₂I₂N₂O₄
Molecular Weight:596.204
Hs Code.:

Synonyms:(S)-1-(1-hydroxy-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propan-2-yl)-3-isopropylurea

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(1-hydroxy-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propan-2-yl)-3-isopropylurea

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Technology Process of (S)-1-(1-hydroxy-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propan-2-yl)-3-isopropylurea

There total 2 articles about (S)-1-(1-hydroxy-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propan-2-yl)-3-isopropylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1380782-27-3
(S)-4-(4-(2-amino-3-hydroxypropyl)-2,6-diiodophenoxy)phenol

: 1795-48-8
Isopropyl isocyanate

: 1417653-80-5
(S)-1-(1-hydroxy-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propan-2-yl)-3-isopropylurea

Guidance literature:: In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;

Reference yield:

: 1041-01-6,534-51-0,5563-89-3,299-82-1
3,5-diiodo-L-thyronine

: 1417653-80-5
(S)-1-(1-hydroxy-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propan-2-yl)-3-isopropylurea

Guidance literature:: Multi-step reaction with 2 steps

1: lithium borohydride; chloro-trimethyl-silane / tetrahydrofuran; 1,4-dioxane / 20 °C / Inert atmosphere; Cooling with ice

2: N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 0 - 20 °C

With lithium borohydride; chloro-trimethyl-silane; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;