6,6-dimethoxy-3-(methoxycarbonyl)-4-methyl-2-methylenecyclohexanecarboxylic acid

Base Information

Chemical Name:6,6-dimethoxy-3-(methoxycarbonyl)-4-methyl-2-methylenecyclohexanecarboxylic acid
CAS No.:107941-50-4
Molecular Formula:C₁₃H₁₈O₆
Molecular Weight:270.282
Hs Code.:

Synonyms:6,6-dimethoxy-3-(methoxycarbonyl)-4-methyl-2-methylenecyclohexanecarboxylic acid

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Chemical Property of 6,6-dimethoxy-3-(methoxycarbonyl)-4-methyl-2-methylenecyclohexanecarboxylic acid

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Technology Process of 6,6-dimethoxy-3-(methoxycarbonyl)-4-methyl-2-methylenecyclohexanecarboxylic acid

There total 2 articles about 6,6-dimethoxy-3-(methoxycarbonyl)-4-methyl-2-methylenecyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 107941-44-6
methyl 8,8-dimethoxy-1,5-dimethyl-3-oxo-2-oxabicyclo<2.2.2>oct-5-ene-6-carboxylate

: 107941-50-4
6,6-dimethoxy-3-(methoxycarbonyl)-4-methyl-2-methylenecyclohexanecarboxylic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; for 1h; Ambient temperature;
DOI:10.1021/jo00386a002

Reference yield:

: 41264-06-6
methyl 4,6-dimethyl-2-oxo-2H-pyran-5-carboxylate

: 107941-50-4
6,6-dimethoxy-3-(methoxycarbonyl)-4-methyl-2-methylenecyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 10 percent / benzene / 24 h / Heating

2: 100 percent / NaOH / tetrahydrofuran; methanol / 1 h / Ambient temperature

With sodium hydroxide; In tetrahydrofuran; methanol; benzene;
DOI:10.1021/jo00386a002