methyl 4-O-(4,6-O-benzylidene-2,3-dideoxy-β-D-erythro-hexopyranosyl)-2,3,6-trideoxy-β-D-erythro-hexopyranoside

Base Information

Chemical Name:methyl 4-O-(4,6-O-benzylidene-2,3-dideoxy-β-D-erythro-hexopyranosyl)-2,3,6-trideoxy-β-D-erythro-hexopyranoside
CAS No.:84094-27-9
Molecular Formula:C₂₀H₂₈O₆
Molecular Weight:364.439
Hs Code.:

Synonyms:methyl 4-O-(4,6-O-benzylidene-2,3-dideoxy-β-D-erythro-hexopyranosyl)-2,3,6-trideoxy-β-D-erythro-hexopyranoside

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Chemical Property of methyl 4-O-(4,6-O-benzylidene-2,3-dideoxy-β-D-erythro-hexopyranosyl)-2,3,6-trideoxy-β-D-erythro-hexopyranoside

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Technology Process of methyl 4-O-(4,6-O-benzylidene-2,3-dideoxy-β-D-erythro-hexopyranosyl)-2,3,6-trideoxy-β-D-erythro-hexopyranoside

There total 9 articles about methyl 4-O-(4,6-O-benzylidene-2,3-dideoxy-β-D-erythro-hexopyranosyl)-2,3,6-trideoxy-β-D-erythro-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 84094-26-8
methyl 4-O-(4,6-O-benzylidene-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl)-2,3,6-trideoxy-β-D-erythro-hex-2-enopyranoside

: 84094-27-9
methyl 4-O-(4,6-O-benzylidene-2,3-dideoxy-β-D-erythro-hexopyranosyl)-2,3,6-trideoxy-β-D-erythro-hexopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In 1,4-dioxane; methanol;
DOI:10.1016/S0008-6215(00)80776-4

Reference yield:

: 84094-24-6
methyl 4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-6-deoxy-β-D-glucopyranoside

: 84094-27-9
methyl 4-O-(4,6-O-benzylidene-2,3-dideoxy-β-D-erythro-hexopyranosyl)-2,3,6-trideoxy-β-D-erythro-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / pyridine / 0 °C

2: 69 percent / NaI, Zn dust / dimethylformamide / 0.5 h / Heating

3: 95 percent / H₂ / 10percent Pd-C / methanol; dioxane

With hydrogen; sodium iodide; zinc; palladium on activated charcoal; In 1,4-dioxane; pyridine; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80776-4

Reference yield:

: Toluene-4-sulfonic acid (2R,3S,4R,5R,6R)-3-((4aR,6S,7R,8R,8aS)-7,8-dihydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-4,5-dihydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester

: 84094-27-9
methyl 4-O-(4,6-O-benzylidene-2,3-dideoxy-β-D-erythro-hexopyranosyl)-2,3,6-trideoxy-β-D-erythro-hexopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / 5 h / Ambient temperature

2: 92 percent / NaI / dimethylformamide / 4 h / 100 °C

3: 85 percent / hydrazine, BaCO₃ / Raney Ni / dioxane; methanol / 0.33 h / Heating

4: 95 percent / 1M NaOMe/MeOH / CHCl₃ / 2 h / Ambient temperature

5: 86 percent / pyridine / 0 °C

6: 69 percent / NaI, Zn dust / dimethylformamide / 0.5 h / Heating

7: 95 percent / H₂ / 10percent Pd-C / methanol; dioxane

With methanol; hydrogen; sodium methylate; barium carbonate; sodium iodide; hydrazine; zinc; palladium on activated charcoal; nickel; In 1,4-dioxane; pyridine; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80776-4