C₂₈H₄₄O₇S

Base Information

Chemical Name:C₂₈H₄₄O₇S
CAS No.:1409941-48-5
Molecular Formula:C₂₈H₄₄O₇S
Molecular Weight:524.719
Hs Code.:

C<sub>28</sub>H<sub>44</sub>O<sub>7</sub>S

Synonyms:C₂₈H₄₄O₇S

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Chemical Property of C₂₈H₄₄O₇S

Chemical Property:

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Technology Process of C₂₈H₄₄O₇S

There total 4 articles about C₂₈H₄₄O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1409941-46-3
C₂₈H₄₆O₅

: 1409941-47-4
C₂₈H₄₄O₇S

: 1409941-48-5
C₂₈H₄₄O₇S

Guidance literature:: C₂₈H₄₆O₅; With thionyl chloride; In tetrachloromethane; at 20 ℃; Inert atmosphere; Reflux;

With sodium periodate; ruthenium(III) chloride trihydrate; In tetrachloromethane; water; acetonitrile; at 0 - 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol302820c

Reference yield:

: 1552-12-1,111-78-4
1,5-cis,cis-cyclooctadiene

: 1409941-48-5
C₂₈H₄₄O₇S

Guidance literature:: Multi-step reaction with 6 steps

1.1: peracetic acid; acetic acid / 0 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: dimethylsulfide borane complex / tetrahydrofuran / -15 - 20 °C / Inert atmosphere

3.1: dimethyl sulfoxide; oxalyl dichloride; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / water; acetone; tert-butyl alcohol / 25 h / 20 °C / Inert atmosphere; Darkness

6.1: thionyl chloride / tetrachloromethane / 20 °C / Inert atmosphere; Reflux

6.2: 48 h / 0 - 20 °C / Inert atmosphere

With peracetic acid; osmium(VIII) oxide; thionyl chloride; oxalyl dichloride; dimethylsulfide borane complex; sodium hexamethyldisilazane; acetic acid; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane; water; acetone; tert-butyl alcohol; 3.1: |Swern Oxidation / 4.1: |Wittig Olefination;
DOI:10.1021/ol302820c

Reference yield:

: 143104-87-4
(4R,5R)-5-(benzyloxy)-7-carboxy-4-heptanolide

: 1409941-48-5
C₂₈H₄₄O₇S

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / -15 - 20 °C / Inert atmosphere

2.1: dimethyl sulfoxide; oxalyl dichloride; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / water; acetone; tert-butyl alcohol / 25 h / 20 °C / Inert atmosphere; Darkness

5.1: thionyl chloride / tetrachloromethane / 20 °C / Inert atmosphere; Reflux

5.2: 48 h / 0 - 20 °C / Inert atmosphere

With osmium(VIII) oxide; thionyl chloride; oxalyl dichloride; dimethylsulfide borane complex; sodium hexamethyldisilazane; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane; water; acetone; tert-butyl alcohol; 2.1: |Swern Oxidation / 3.1: |Wittig Olefination;
DOI:10.1021/ol302820c