N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin-farnesylester

Base Information

Chemical Name:N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin-farnesylester
CAS No.:103669-56-3
Molecular Formula:C₃₉H₅₃NO₁₃
Molecular Weight:743.849
Hs Code.:

Synonyms:N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin-farnesylester

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Chemical Property of N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin-farnesylester

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Technology Process of N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin-farnesylester

There total 4 articles about N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin-farnesylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.5%

: 103670-05-9
DL-2-Phenylglycin-farnesylester-hydrochlorid

: 103670-01-5
2,3-Dihydro-3-oxo-4-(2,3,4,5,6-penta-O-acetyl-D-gluconoyloxy)-2,5-diphenylthiophen-1,1-dioxid

: 103669-56-3
N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin-farnesylester

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃;

Reference yield:

: 17430-71-6
penta-O-acetyl-D-gluconic acid

: 103669-56-3
N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin-farnesylester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / pyridine / CH₂Cl₂ / 2 h / 25 °C

2: 89.5 percent / triethylamine / CH₂Cl₂ / 25 °C

With pyridine; triethylamine; In dichloromethane;

Reference yield:

: 24163-93-7,24163-94-8,28290-41-7,56881-57-3,6874-67-5
farnesyl bromide

: 103669-56-3
N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin-farnesylester

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) HCl / 1.) THF, 15 h, reflux 2.) ether, 1 h, -78 deg C

2: 89.5 percent / triethylamine / CH₂Cl₂ / 25 °C

With hydrogenchloride; triethylamine; In dichloromethane;