methyl 6-exo-3-oxo-6-(phenylseleno)bicyclo<3.3.1>nonane-1-dicarboxylate

Base Information

Chemical Name:methyl 6-exo-3-oxo-6-(phenylseleno)bicyclo<3.3.1>nonane-1-dicarboxylate
CAS No.:114584-49-5
Molecular Formula:C₁₇H₂₀O₃Se
Molecular Weight:351.304
Hs Code.:

Synonyms:methyl 6-exo-3-oxo-6-(phenylseleno)bicyclo<3.3.1>nonane-1-dicarboxylate

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Chemical Property of methyl 6-exo-3-oxo-6-(phenylseleno)bicyclo<3.3.1>nonane-1-dicarboxylate

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Technology Process of methyl 6-exo-3-oxo-6-(phenylseleno)bicyclo<3.3.1>nonane-1-dicarboxylate

There total 4 articles about methyl 6-exo-3-oxo-6-(phenylseleno)bicyclo<3.3.1>nonane-1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 114584-48-4
6-exo-3-oxo-6-(phenylseleno)bicyclo<3.3.1>nonane-1,4-dicarboxylic acid 1-methyl 4-ethyl diester

: 114584-49-5
methyl 6-exo-3-oxo-6-(phenylseleno)bicyclo<3.3.1>nonane-1-dicarboxylate

Guidance literature:: With water; dimethyl sulfoxide; at 150 ℃; for 3.25h;
DOI:10.1021/jo00249a013

Reference yield:

: 52251-58-8
lithium phenylselenide

: 114584-49-5
methyl 6-exo-3-oxo-6-(phenylseleno)bicyclo<3.3.1>nonane-1-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.5 h / 0 °C

2: 74 percent / DMSO, H₂O / 3.25 h / 150 °C

With water; dimethyl sulfoxide; In tetrahydrofuran;
DOI:10.1021/jo00249a013

Reference yield:

: 114595-86-7
3-oxotricyclo<3.3.1.0^2,8>nonane-2,5-dicarboxylic acid 2-ethyl 5-methyl diester

: 114584-49-5
methyl 6-exo-3-oxo-6-(phenylseleno)bicyclo<3.3.1>nonane-1-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.5 h / 0 °C

2: 74 percent / DMSO, H₂O / 3.25 h / 150 °C

With water; dimethyl sulfoxide; In tetrahydrofuran;
DOI:10.1021/jo00249a013