(+/-)-trans-2-(3,4-dimethoxyphenyl)-2,3-dihydro-5-allyl-6-(allyloxy)-3-methylbenzofuran

Base Information

Chemical Name:(+/-)-trans-2-(3,4-dimethoxyphenyl)-2,3-dihydro-5-allyl-6-(allyloxy)-3-methylbenzofuran
CAS No.:132802-72-3
Molecular Formula:C₂₃H₂₆O₄
Molecular Weight:366.457
Hs Code.:

Synonyms:(+/-)-trans-2-(3,4-dimethoxyphenyl)-2,3-dihydro-5-allyl-6-(allyloxy)-3-methylbenzofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-trans-2-(3,4-dimethoxyphenyl)-2,3-dihydro-5-allyl-6-(allyloxy)-3-methylbenzofuran

Chemical Property:

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Technology Process of (+/-)-trans-2-(3,4-dimethoxyphenyl)-2,3-dihydro-5-allyl-6-(allyloxy)-3-methylbenzofuran

There total 6 articles about (+/-)-trans-2-(3,4-dimethoxyphenyl)-2,3-dihydro-5-allyl-6-(allyloxy)-3-methylbenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 6379-72-2
1,2-dimethoxy-4-(E)-propenylbenzene

: 132802-71-2
4-allyl-3-(allyloxy)phenol

: 132802-72-3
(+/-)-trans-2-(3,4-dimethoxyphenyl)-2,3-dihydro-5-allyl-6-(allyloxy)-3-methylbenzofuran

Guidance literature:: With bis-[(trifluoroacetoxy)iodo]benzene; In acetonitrile; a) 0 deg C, 20 min, b) r.t., 20 min;
DOI:10.1021/jo00033a040

Reference yield:

: 132802-62-1
1-(tert-Butyldimethylsiloxy)-3-(allyloxy)benzene

: 132802-72-3
(+/-)-trans-2-(3,4-dimethoxyphenyl)-2,3-dihydro-5-allyl-6-(allyloxy)-3-methylbenzofuran

Guidance literature:: Multi-step reaction with 2 steps

2: 32 percent / iodobenzene bis(trifluoroacetate) / acetonitrile / a) 0 deg C, 20 min, b) r.t., 20 min

With bis-[(trifluoroacetoxy)iodo]benzene; In acetonitrile;
DOI:10.1021/jo00033a040

Reference yield:

: 1616-51-9
3-allyloxyphenol

: 132802-72-3
(+/-)-trans-2-(3,4-dimethoxyphenyl)-2,3-dihydro-5-allyl-6-(allyloxy)-3-methylbenzofuran

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / imidazole / acetonitrile / 2 h / Ambient temperature

3: 32 percent / iodobenzene bis(trifluoroacetate) / acetonitrile / a) 0 deg C, 20 min, b) r.t., 20 min

With 1H-imidazole; bis-[(trifluoroacetoxy)iodo]benzene; In acetonitrile;
DOI:10.1021/jo00033a040