phenyl 6-O-benzoyl-4-O-benzyl-2,3-dideoxy-1-thio-α-D-erythro-hexopyranoside

Base Information

Chemical Name:phenyl 6-O-benzoyl-4-O-benzyl-2,3-dideoxy-1-thio-α-D-erythro-hexopyranoside
CAS No.:1301176-58-8
Molecular Formula:C₂₆H₂₆O₄S
Molecular Weight:434.556
Hs Code.:

Synonyms:phenyl 6-O-benzoyl-4-O-benzyl-2,3-dideoxy-1-thio-α-D-erythro-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 6-O-benzoyl-4-O-benzyl-2,3-dideoxy-1-thio-α-D-erythro-hexopyranoside

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Technology Process of phenyl 6-O-benzoyl-4-O-benzyl-2,3-dideoxy-1-thio-α-D-erythro-hexopyranoside

There total 1 articles about phenyl 6-O-benzoyl-4-O-benzyl-2,3-dideoxy-1-thio-α-D-erythro-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1221720-91-7
6-O-benzoyl-4-O-benzyl-2,3-dideoxy-α-D-erythro-hexopyranosyl acetate

: 108-98-5
thiophenol

: 1301176-58-8
phenyl 6-O-benzoyl-4-O-benzyl-2,3-dideoxy-1-thio-α-D-erythro-hexopyranoside

: 1301176-60-2
phenyl 6-O-benzoyl-4-O-benzyl-2,3-dideoxy-1-thio-β-D-erythro-hexopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -50 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.02.109

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 1301176-58-8
phenyl 6-O-benzoyl-4-O-benzyl-2,3-dideoxy-1-thio-α-D-erythro-hexopyranoside

: 1221720-93-9
methyl 6-O-(6'-O-benzoyl-4'-O-benzyl-2',3'-dideoxy-α-D-erythro-hexopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 1221720-95-1
methyl 6-O-(6'-O-benzoyl-4'-O-benzyl-2',3'-dideoxy-β-D-erythro-hexopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: methyl 2,3,4-tri-O-benzyl-D-glucopyranoside; phenyl 6-O-benzoyl-4-O-benzyl-2,3-dideoxy-1-thio-α-D-erythro-hexopyranoside; With phenyl 4,6-O-di-benzoyl-2,3-dideoxy-1-thio-D-erythro-hexopyranoside; In dichloromethane; at 25 ℃; for 0.5h; Molecular sieve;

With N-Bromosuccinimide; In dichloromethane; at -45 ℃; for 3h; optical yield given as %de; chemoselective reaction;
DOI:10.1016/j.tetlet.2011.02.109