2-Phenyl-2-(tetraphenylcyclopentadienyl)ethyl Trifluoromethanesulfonate

Base Information

• Chemical Name: 2-Phenyl-2-(tetraphenylcyclopentadienyl)ethyl Trifluoromethanesulfonate
• CAS No.: 143007-38-9
• Molecular Formula: C₃₈H₂₉F₃O₃S
• Molecular Weight: 622.708

Synonyms:2-Phenyl-2-(tetraphenylcyclopentadienyl)ethyl Trifluoromethanesulfonate

Chemical Property of 2-Phenyl-2-(tetraphenylcyclopentadienyl)ethyl Trifluoromethanesulfonate

Chemical Property:

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Technology Process of 2-Phenyl-2-(tetraphenylcyclopentadienyl)ethyl Trifluoromethanesulfonate

There total 1 articles about 2-Phenyl-2-(tetraphenylcyclopentadienyl)ethyl Trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

trifluoromethylsulfonic anhydride (358-23-6) + 2-Phenyl-2-(tetraphenylcyclopentadienyl)ethanol (143007-34-5) → 2-Phenyl-2-(tetraphenylcyclopentadienyl)ethyl Trifluoromethanesulfonate (143007-38-9)

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; for 0.25h;

Reference yield: 65.0%

cyclopentadienylsodium*dioxane + 2-Phenyl-2-(tetraphenylcyclopentadienyl)ethyl Trifluoromethanesulfonate (143007-38-9) → 1-(1-cyclopentadienyl)-1-phenyl-2-(1,2,3,4-tetraphenyl-5-cyclopentadienyl)ethane (143007-40-3)

Guidance literature:

In N,N-dimethyl-formamide; at -20 ℃; for 72h;

Reference yield:

1,2,3,4-tetraphenylcyclopentadiene (15570-45-3) + 2-Phenyl-2-(tetraphenylcyclopentadienyl)ethyl Trifluoromethanesulfonate (143007-38-9) → 1-Phenyl-1,2-bis(tetraphenylcyclopentadienyl)ethane

Guidance literature:

Yield given. Multistep reaction; DMF;

upstream raw materials:

trifluoromethylsulfonic anhydride

2-Phenyl-2-(tetraphenylcyclopentadienyl)ethanol

Downstream raw materials:

1-(1-cyclopentadienyl)-1-phenyl-2-(1,2,3,4-tetraphenyl-5-cyclopentadienyl)ethane

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