phenyl 6-O-acetyl-3-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 6-O-acetyl-3-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside
CAS No.:79528-54-4
Molecular Formula:C₂₉H₂₇NO₇S
Molecular Weight:533.602
Hs Code.:

Synonyms:phenyl 6-O-acetyl-3-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 6-O-acetyl-3-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 6-O-acetyl-3-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

There total 7 articles about phenyl 6-O-acetyl-3-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 108-24-7
acetic anhydride

: 79528-53-3
phenyl 3-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 79528-54-4
phenyl 6-O-acetyl-3-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; In 1,2-dichloro-ethane; at 5 ℃; for 1.5h;
DOI:10.1016/S0008-6215(00)85587-1

Reference yield:

: 10022-13-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

: 79528-54-4
phenyl 6-O-acetyl-3-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 65 percent / SnCl₄ / 1,2-dichloro-ethane / 10 h / 25 °C

2: aq. HCl / acetone / 3 h / 50 - 60 °C

3: TsOH*H₂O / acetonitrile / 15 h / 20 °C

4: NaH / dimethylformamide / 15 h / 20 °C

5: aq. acetic acid / 0.75 h / 100 °C

6: 56 percent / pyridine / 1,2-dichloro-ethane / 1.5 h / 5 °C

With pyridine; hydrogenchloride; tin(IV) chloride; sodium hydride; toluene-4-sulfonic acid; acetic acid; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/S0008-6215(00)85587-1

Reference yield:

: 17314-33-9
tributyltin phenyl sulfide

: 79528-54-4
phenyl 6-O-acetyl-3-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 65 percent / SnCl₄ / 1,2-dichloro-ethane / 10 h / 25 °C

2: aq. HCl / acetone / 3 h / 50 - 60 °C

3: TsOH*H₂O / acetonitrile / 15 h / 20 °C

4: NaH / dimethylformamide / 15 h / 20 °C

5: aq. acetic acid / 0.75 h / 100 °C

6: 56 percent / pyridine / 1,2-dichloro-ethane / 1.5 h / 5 °C

With pyridine; hydrogenchloride; tin(IV) chloride; sodium hydride; toluene-4-sulfonic acid; acetic acid; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/S0008-6215(00)85587-1