methyl 4'-[11-(1-methylcyclobutan-1-ylmethoxy)undecyloxy]biphenyl-4-carboxylate

Base Information

Chemical Name:methyl 4'-[11-(1-methylcyclobutan-1-ylmethoxy)undecyloxy]biphenyl-4-carboxylate
CAS No.:915710-16-6
Molecular Formula:C₃₁H₄₄O₄
Molecular Weight:480.688
Hs Code.:

Synonyms:methyl 4'-[11-(1-methylcyclobutan-1-ylmethoxy)undecyloxy]biphenyl-4-carboxylate

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Chemical Property of methyl 4'-[11-(1-methylcyclobutan-1-ylmethoxy)undecyloxy]biphenyl-4-carboxylate

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Technology Process of methyl 4'-[11-(1-methylcyclobutan-1-ylmethoxy)undecyloxy]biphenyl-4-carboxylate

There total 4 articles about methyl 4'-[11-(1-methylcyclobutan-1-ylmethoxy)undecyloxy]biphenyl-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 915710-11-1
1-(11-bromoundecyloxymethyl)-1-methylcyclobutane

: 40501-41-5
methyl 4'-hydroxy-4-biphenylcarboxylate

: 915710-16-6
methyl 4'-[11-(1-methylcyclobutan-1-ylmethoxy)undecyloxy]biphenyl-4-carboxylate

Guidance literature:: With potassium carbonate; In butanone; Heating;
DOI:10.1039/b610154b

Reference yield:

: 3721-95-7
Cyclobutanecarboxylic acid

: 915710-16-6
methyl 4'-[11-(1-methylcyclobutan-1-ylmethoxy)undecyloxy]biphenyl-4-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: LDA / tetrahydrofuran; hexane / 0.25 h / 5 °C

1.2: 95 percent / tetrahydrofuran; hexane / 20 °C

2.1: 85 percent / lithium aluminium hydride / diethyl ether / 3 h / Heating

3.1: 29 percent / aq. sodium hydroxide; tetrabutylammonium bromide / hexane / 3 h / Heating

4.1: 73 percent / potassium carbonate / butan-2-one / Heating

With sodium hydroxide; lithium aluminium tetrahydride; tetrabutylammomium bromide; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; butanone;
DOI:10.1039/b610154b

Reference yield:

: 32936-76-8
1-methylcyclobutane carboxylic acid

: 915710-16-6
methyl 4'-[11-(1-methylcyclobutan-1-ylmethoxy)undecyloxy]biphenyl-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / lithium aluminium hydride / diethyl ether / 3 h / Heating

2: 29 percent / aq. sodium hydroxide; tetrabutylammonium bromide / hexane / 3 h / Heating

3: 73 percent / potassium carbonate / butan-2-one / Heating

With sodium hydroxide; lithium aluminium tetrahydride; tetrabutylammomium bromide; potassium carbonate; In diethyl ether; hexane; butanone;
DOI:10.1039/b610154b